<3--5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>carbamic acid 1,1-dimethylethyl ester

Base Information

Chemical Name:<3--5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>carbamic acid 1,1-dimethylethyl ester
CAS No.:147355-07-5
Molecular Formula:C₃₂H₃₅BrClN₇O₃
Molecular Weight:681.032
Hs Code.:

<3-<N-<2-<(4-amino-6-chloro-1,3,5-triazin-2-yl)amino>-5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>carbamic acid 1,1-dimethylethyl ester

Synonyms:<3--5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>carbamic acid 1,1-dimethylethyl ester

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Chemical Property of <3--5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>carbamic acid 1,1-dimethylethyl ester

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Technology Process of <3--5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>carbamic acid 1,1-dimethylethyl ester

There total 10 articles about <3--5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>carbamic acid 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: {3-[[5-Bromo-2-(4,6-dichloro-[1,3,5]triazin-2-ylamino)-benzoyl]-(4-tert-butyl-benzyl)-amino]-phenyl}-carbamic acid tert-butyl ester

: 147355-07-5
<3--5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>carbamic acid 1,1-dimethylethyl ester

Guidance literature:: With ammonia; In tetrahydrofuran; at 0 ℃; for 1h; Yield given;
DOI:10.1021/ja00056a014

Reference yield:

: 68621-88-5
(3-aminophenyl)carbamic acid tert-butyl ester

: 147355-07-5
<3--5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>carbamic acid 1,1-dimethylethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 68 percent / triethylamine / tetrahydrofuran / 12 h / Heating

2: 90 percent / triethylamine / CH₂Cl₂; toluene / 1 h / Ambient temperature

3: 95 percent / hydrazine / methanol / 4 h / Heating

4: diisopropylethylamine / tetrahydrofuran / 1 h / 0 °C

5: NH₃ gas / tetrahydrofuran / 1 h / 0 °C

With ammonia; triethylamine; N-ethyl-N,N-diisopropylamine; hydrazine; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/ja00056a014

Reference yield:

: 147355-04-2
5-bromo-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)benzoic acid

: 147355-07-5
<3--5-bromobenzoyl>-N-<<4-(1,1-dimethylethyl)phenyl>methyl>amino>phenyl>carbamic acid 1,1-dimethylethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride / 2 h / Heating

2: 90 percent / triethylamine / CH₂Cl₂; toluene / 1 h / Ambient temperature

3: 95 percent / hydrazine / methanol / 4 h / Heating

4: diisopropylethylamine / tetrahydrofuran / 1 h / 0 °C

5: NH₃ gas / tetrahydrofuran / 1 h / 0 °C

With thionyl chloride; ammonia; triethylamine; N-ethyl-N,N-diisopropylamine; hydrazine; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/ja00056a014