(Z)-4-[(1R,5R,6R)-6-dimethoxymethyl-5-isopropyl-2-methyl-cyclohex-2-enyl]-2-methyl-but-2-en-1-ol

Base Information

Chemical Name:(Z)-4-[(1R,5R,6R)-6-dimethoxymethyl-5-isopropyl-2-methyl-cyclohex-2-enyl]-2-methyl-but-2-en-1-ol
CAS No.:221290-58-0
Molecular Formula:C₁₈H₃₂O₃
Molecular Weight:296.45
Hs Code.:

Synonyms:(Z)-4-[(1R,5R,6R)-6-dimethoxymethyl-5-isopropyl-2-methyl-cyclohex-2-enyl]-2-methyl-but-2-en-1-ol

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Chemical Property of (Z)-4-[(1R,5R,6R)-6-dimethoxymethyl-5-isopropyl-2-methyl-cyclohex-2-enyl]-2-methyl-but-2-en-1-ol

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Technology Process of (Z)-4-[(1R,5R,6R)-6-dimethoxymethyl-5-isopropyl-2-methyl-cyclohex-2-enyl]-2-methyl-but-2-en-1-ol

There total 15 articles about (Z)-4-[(1R,5R,6R)-6-dimethoxymethyl-5-isopropyl-2-methyl-cyclohex-2-enyl]-2-methyl-but-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 380414-33-5
(Z)-4-[(1R,5R,6R)-6-dimethoxymethyl-5-isopropyl-2-methyl-cyclohex-2-enyl]-2-methyl-but-2-enoic acid

: 221290-58-0
(Z)-4-[(1R,5R,6R)-6-dimethoxymethyl-5-isopropyl-2-methyl-cyclohex-2-enyl]-2-methyl-but-2-en-1-ol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; Ambient temperature;
DOI:10.1016/S0040-4039(98)80045-2

Reference yield: 72.0%

: 380414-34-6
(E)-4-[(1R,5R,6R)-6-dimethoxymethyl-5-isopropyl-2-methyl-cyclohex-2-enyl]-2-methyl-but-2-enoic acid

: 221290-58-0
(Z)-4-[(1R,5R,6R)-6-dimethoxymethyl-5-isopropyl-2-methyl-cyclohex-2-enyl]-2-methyl-but-2-en-1-ol

: 221290-59-1
(E)-4-[(1R,5R,6R)-6-dimethoxymethyl-5-isopropyl-2-methyl-cyclohex-2-enyl]-2-methyl-but-2-en-1-ol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 - 20 ℃; for 1h;
DOI:10.1016/S0040-4020(01)00739-6

Reference yield:

: 221290-56-8
[(1R,5R,6R)-6-dimethoxymethyl-5-isopropyl-2-methyl-cyclohex-2-enyl]-acetic acid

: 221290-58-0
(Z)-4-[(1R,5R,6R)-6-dimethoxymethyl-5-isopropyl-2-methyl-cyclohex-2-enyl]-2-methyl-but-2-en-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / LiAlH₄ / diethyl ether / 2 h / 0 - 20 °C

2: 97 percent / Dess-Martin periodinane / CH₂Cl₂ / 30 h / 20 °C

3: NaH / 1,2-dimethoxy-ethane / 1 h / 20 °C

4: 92 percent / LiAlH₄ / diethyl ether / 1 h / 0 - 20 °C

With lithium aluminium tetrahydride; sodium hydride; Dess-Martin periodane; In 1,2-dimethoxyethane; diethyl ether; dichloromethane; 3: Horner-Emmons reaction;
DOI:10.1016/S0040-4020(01)00739-6