2-(3-benzyloxy-1,4,5,6,8-pentamethoxynaphthalen-2-yl)-5,5-dimethyl-1,3-dioxane

Base Information

Chemical Name:2-(3-benzyloxy-1,4,5,6,8-pentamethoxynaphthalen-2-yl)-5,5-dimethyl-1,3-dioxane
CAS No.:916755-19-6
Molecular Formula:C₂₈H₃₄O₈
Molecular Weight:498.573
Hs Code.:

Synonyms:2-(3-benzyloxy-1,4,5,6,8-pentamethoxynaphthalen-2-yl)-5,5-dimethyl-1,3-dioxane

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Chemical Property of 2-(3-benzyloxy-1,4,5,6,8-pentamethoxynaphthalen-2-yl)-5,5-dimethyl-1,3-dioxane

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Technology Process of 2-(3-benzyloxy-1,4,5,6,8-pentamethoxynaphthalen-2-yl)-5,5-dimethyl-1,3-dioxane

There total 2 articles about 2-(3-benzyloxy-1,4,5,6,8-pentamethoxynaphthalen-2-yl)-5,5-dimethyl-1,3-dioxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7-benzyloxy-6-(5,5-dimethyl-[1,3]dioxan-2-yl)-1,4,5,8-tetramethoxy-naphthalen-2-ol

: 77-78-1
dimethyl sulfate

: 2-(3-benzyloxy-1,4,5,8-tetramethoxynaphthalen-2-yl)-5,5-dimethyl-1,3-dioxane

: 916755-19-6
2-(3-benzyloxy-1,4,5,6,8-pentamethoxynaphthalen-2-yl)-5,5-dimethyl-1,3-dioxane

Guidance literature:: With sodium hydroxide; tetrabutylammomium bromide; In dichloromethane; water; at 20 ℃; for 20h;
DOI:10.1002/ejoc.200600353

Reference yield:

: C₂₇H₃₃BO₉

: 916755-19-6
2-(3-benzyloxy-1,4,5,6,8-pentamethoxynaphthalen-2-yl)-5,5-dimethyl-1,3-dioxane

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen peroxide; sodium hydroxide / H₂O; methanol / 0.17 h / 20 °C

2: 261 mg / tetra-n-butylammonium bromide; sodium hydroxide / CH₂Cl₂; H₂O / 20 h / 20 °C

With sodium hydroxide; tetrabutylammomium bromide; dihydrogen peroxide; In methanol; dichloromethane; water;
DOI:10.1002/ejoc.200600353