10-methyl-9-{4-[4-(1,4,7,10,13-pentaoxa-16-azacyclooctadecan-16-yl)phenyl]-1H-1,2,3-triazol-1-yl}methylanthracene

Base Information

Chemical Name:10-methyl-9-{4-[4-(1,4,7,10,13-pentaoxa-16-azacyclooctadecan-16-yl)phenyl]-1H-1,2,3-triazol-1-yl}methylanthracene
CAS No.:1441687-51-9
Molecular Formula:C₃₆H₄₂N₄O₅
Molecular Weight:610.753
Hs Code.:

Synonyms:10-methyl-9-{4-[4-(1,4,7,10,13-pentaoxa-16-azacyclooctadecan-16-yl)phenyl]-1H-1,2,3-triazol-1-yl}methylanthracene

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Chemical Property of 10-methyl-9-{4-[4-(1,4,7,10,13-pentaoxa-16-azacyclooctadecan-16-yl)phenyl]-1H-1,2,3-triazol-1-yl}methylanthracene

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Technology Process of 10-methyl-9-{4-[4-(1,4,7,10,13-pentaoxa-16-azacyclooctadecan-16-yl)phenyl]-1H-1,2,3-triazol-1-yl}methylanthracene

There total 3 articles about 10-methyl-9-{4-[4-(1,4,7,10,13-pentaoxa-16-azacyclooctadecan-16-yl)phenyl]-1H-1,2,3-triazol-1-yl}methylanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1304015-88-0
N-(4-ethynylphenyl)-1-aza-[18]crown-6 ether

: 1398940-12-9
9-azidomethyl-10-methylanthracene

: 1441687-51-9
10-methyl-9-{4-[4-(1,4,7,10,13-pentaoxa-16-azacyclooctadecan-16-yl)phenyl]-1H-1,2,3-triazol-1-yl}methylanthracene

Guidance literature:: With copper nanoparticles on activated carbon; triethylamine; In tetrahydrofuran; at 60 ℃; for 64h;
DOI:10.1002/chem.201201575

Reference yield:

: 34331-95-8
9-bromomethyl-10-methylanthracene

: 1441687-51-9
10-methyl-9-{4-[4-(1,4,7,10,13-pentaoxa-16-azacyclooctadecan-16-yl)phenyl]-1H-1,2,3-triazol-1-yl}methylanthracene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / acetonitrile / 5 h / Reflux

2: copper nanoparticles on activated carbon; triethylamine / tetrahydrofuran / 64 h / 60 °C

With sodium azide; copper nanoparticles on activated carbon; triethylamine; In tetrahydrofuran; acetonitrile;
DOI:10.1002/chem.201201575

Reference yield:

: 9,10-dihydroxy-9,10-dimethylanthracene

: 1441687-51-9
10-methyl-9-{4-[4-(1,4,7,10,13-pentaoxa-16-azacyclooctadecan-16-yl)phenyl]-1H-1,2,3-triazol-1-yl}methylanthracene

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen bromide / tetrahydrofuran / 0.5 h / 20 °C

2: sodium azide / acetonitrile / 5 h / Reflux

3: copper nanoparticles on activated carbon; triethylamine / tetrahydrofuran / 64 h / 60 °C

With sodium azide; copper nanoparticles on activated carbon; hydrogen bromide; triethylamine; In tetrahydrofuran; acetonitrile;
DOI:10.1002/chem.201201575