2-[4-(4-tert-butoxycarbonylaminobenzyl)phenylimino]imidazolidine-1,3-dicarboxylic acid di-tert-butyl ester

Base Information

• Chemical Name: 2-[4-(4-tert-butoxycarbonylaminobenzyl)phenylimino]imidazolidine-1,3-dicarboxylic acid di-tert-butyl ester
• CAS No.: 1196966-39-8
• Molecular Formula: C₃₁H₄₂N₄O₆
• Molecular Weight: 566.698

Synonyms:2-[4-(4-tert-butoxycarbonylaminobenzyl)phenylimino]imidazolidine-1,3-dicarboxylic acid di-tert-butyl ester

Chemical Property of 2-[4-(4-tert-butoxycarbonylaminobenzyl)phenylimino]imidazolidine-1,3-dicarboxylic acid di-tert-butyl ester

Chemical Property:

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Technology Process of 2-[4-(4-tert-butoxycarbonylaminobenzyl)phenylimino]imidazolidine-1,3-dicarboxylic acid di-tert-butyl ester

There total 1 articles about 2-[4-(4-tert-butoxycarbonylaminobenzyl)phenylimino]imidazolidine-1,3-dicarboxylic acid di-tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

N-{4-[(4-aminobenzyl)phenyl]}carbamic acid 1,1-dimethylethyl ester (135680-03-4) + 2-thioxo-imidazolidine-1,3-dicarboxylic acid di-tert-butyl ester (173300-83-9) → 2-[4-(4-tert-butoxycarbonylaminobenzyl)phenylimino]imidazolidine-1,3-dicarboxylic acid di-tert-butyl ester (1196966-39-8)

Guidance literature:

With triethylamine; mercury dichloride; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/jm901017t

Reference yield:

2-[4-(4-tert-butoxycarbonylaminobenzyl)phenylimino]imidazolidine-1,3-dicarboxylic acid di-tert-butyl ester (1196966-39-8) + trifluoroacetic acid (76-05-1) → 2-[4-(4-aminobenzyl)phenylimino]imidazolidine bis(trifluoroacetate)

Guidance literature:

In dichloromethane; at 20 ℃; for 3h;

DOI:10.1021/jm901017t

upstream raw materials:

N-{4-[(4-aminobenzyl)phenyl]}carbamic acid 1,1-dimethylethyl ester

2-thioxo-imidazolidine-1,3-dicarboxylic acid di-tert-butyl ester

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