3-[2-(4-fluorophenyl)vinyl]-2-quinoxalinyl phenyl sulfide

Base Information

Chemical Name:3-[2-(4-fluorophenyl)vinyl]-2-quinoxalinyl phenyl sulfide
CAS No.:366018-63-5
Molecular Formula:C₂₂H₁₅FN₂S
Molecular Weight:358.439
Hs Code.:
Mol file:366018-63-5.mol

Synonyms:2-[(E)-2-(4-Fluoro-phenyl)-vinyl]-3-phenylsulfanyl-quinoxaline

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Chemical Property of 3-[2-(4-fluorophenyl)vinyl]-2-quinoxalinyl phenyl sulfide

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Technology Process of 3-[2-(4-fluorophenyl)vinyl]-2-quinoxalinyl phenyl sulfide

There total 4 articles about 3-[2-(4-fluorophenyl)vinyl]-2-quinoxalinyl phenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 108-98-5
thiophenol

: 53047-15-7
2-Chloro-3-[(E)-2-(4-fluoro-phenyl)-vinyl]-quinoxaline

: 366018-63-5
2-[(E)-2-(4-Fluoro-phenyl)-vinyl]-3-phenylsulfanyl-quinoxaline

Guidance literature:: With triethylamine; In methanol; Heating;

Reference yield:

: 14003-34-0
3-methyl-2-oxo-1,2-dihydroquinoxaline

: 366018-63-5
2-[(E)-2-(4-Fluoro-phenyl)-vinyl]-3-phenylsulfanyl-quinoxaline

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / 3 h / 180 °C

2: 93.5 percent / DMF; POCl₃ / 0.75 h / 105 °C

3: 93 percent / Et₃N / methanol / Heating

With triethylamine; N,N-dimethyl-formamide; trichlorophosphate; In methanol;

Reference yield:

: 95-54-5
1,2-diamino-benzene

: 366018-63-5
2-[(E)-2-(4-Fluoro-phenyl)-vinyl]-3-phenylsulfanyl-quinoxaline

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / HCl / H₂O / 0.25 h / 20 °C

2: 95 percent / 3 h / 180 °C

3: 93.5 percent / DMF; POCl₃ / 0.75 h / 105 °C

4: 93 percent / Et₃N / methanol / Heating

With hydrogenchloride; triethylamine; N,N-dimethyl-formamide; trichlorophosphate; In methanol; water;