C₄₆H₄₉O₁₁P

Base Information

Chemical Name:C₄₆H₄₉O₁₁P
CAS No.:1428872-88-1
Molecular Formula:C₄₆H₄₉O₁₁P
Molecular Weight:808.862
Hs Code.:

C<sub>46</sub>H<sub>49</sub>O<sub>11</sub>P

Synonyms:C₄₆H₄₉O₁₁P

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Chemical Property of C₄₆H₄₉O₁₁P

Chemical Property:

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Technology Process of C₄₆H₄₉O₁₁P

There total 5 articles about C₄₆H₄₉O₁₁P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₆H₄₉O₁₀P

: 1428872-88-1
C₄₆H₄₉O₁₁P

Guidance literature:: With tert.-butylhydroperoxide; In water; at 20 ℃; for 1h;
DOI:10.1016/j.bmcl.2013.02.068

Reference yield:

: 93451-41-3
allyl-2,3,4-tri-O-benzyl-6-O-trityl-α-D-mannopyranoside

: 1428872-88-1
C₄₆H₄₉O₁₁P

Guidance literature:: Multi-step reaction with 5 steps

1.1: ruthenium trichloride; sodium periodate / dichloromethane; acetonitrile; water / 2 h / 20 °C

2.1: potassium carbonate / dichloromethane / 6 h / 20 °C

3.1: iron(III) chloride hexahydrate / dichloromethane / 2 h / 0 - 20 °C

4.1: 1H-tetrazole / dichloromethane; acetonitrile / 2 h / 20 °C / Molecular sieve; Inert atmosphere

4.2: 3 h / 20 °C / Molecular sieve; Inert atmosphere

5.1: tert.-butylhydroperoxide / water / 1 h / 20 °C

With 1H-tetrazole; tert.-butylhydroperoxide; ruthenium trichloride; sodium periodate; iron(III) chloride hexahydrate; potassium carbonate; In dichloromethane; water; acetonitrile;
DOI:10.1016/j.bmcl.2013.02.068

Reference yield:

: ((2S,3S,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-trityloxymethyl-tetrahydro-pyran-2-yloxy)-acetic acid

: 1428872-88-1
C₄₆H₄₉O₁₁P

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / dichloromethane / 6 h / 20 °C

2.1: iron(III) chloride hexahydrate / dichloromethane / 2 h / 0 - 20 °C

3.1: 1H-tetrazole / dichloromethane; acetonitrile / 2 h / 20 °C / Molecular sieve; Inert atmosphere

3.2: 3 h / 20 °C / Molecular sieve; Inert atmosphere

4.1: tert.-butylhydroperoxide / water / 1 h / 20 °C

With 1H-tetrazole; tert.-butylhydroperoxide; iron(III) chloride hexahydrate; potassium carbonate; In dichloromethane; water; acetonitrile;
DOI:10.1016/j.bmcl.2013.02.068