1,3-bis(2,3,4,5,6-pentamethylbenzyl)-1H-benzo[d]imidazol-3-ium chloride

Base Information

Chemical Name:1,3-bis(2,3,4,5,6-pentamethylbenzyl)-1H-benzo[d]imidazol-3-ium chloride
CAS No.:1231749-85-1
Molecular Formula:C₃₁H₃₉N₂*Cl
Molecular Weight:475.117
Hs Code.:

Synonyms:1,3-bis(2,3,4,5,6-pentamethylbenzyl)-1H-benzo[d]imidazol-3-ium chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-bis(2,3,4,5,6-pentamethylbenzyl)-1H-benzo[d]imidazol-3-ium chloride

Chemical Property:

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Technology Process of 1,3-bis(2,3,4,5,6-pentamethylbenzyl)-1H-benzo[d]imidazol-3-ium chloride

There total 3 articles about 1,3-bis(2,3,4,5,6-pentamethylbenzyl)-1H-benzo[d]imidazol-3-ium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1-(2,3,4,5,6-pentamethylbenzyl)-1H-benzo[d]imidazole

: 484-65-1
2,3,4,5,6-pentamethylbenzyl chloride

: 1231749-85-1
1,3-bis(2,3,4,5,6-pentamethylbenzyl)-1H-benzo[d]imidazol-3-ium chloride

Guidance literature:: In N,N-dimethyl-formamide; at 70 ℃;
DOI:10.1016/j.ica.2017.06.065

Reference yield:

: 51-17-2,79351-71-6
benzoimidazole

: 1231749-85-1
1,3-bis(2,3,4,5,6-pentamethylbenzyl)-1H-benzo[d]imidazol-3-ium chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / ethanol / 1 h / 20 °C / Inert atmosphere; Schlenk technique

1.2: 80 °C / Inert atmosphere; Schlenk technique

2.1: N,N-dimethyl-formamide / 70 °C

With potassium hydroxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ica.2017.06.065

Reference yield:

: 484-65-1
2,3,4,5,6-pentamethylbenzyl chloride

: 1231749-85-1
1,3-bis(2,3,4,5,6-pentamethylbenzyl)-1H-benzo[d]imidazol-3-ium chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / ethanol / 0.25 h / 20 °C

1.2: 17 h / 20 °C / Reflux

2.1: N,N-dimethyl-formamide / 70 °C / Schlenk technique

With potassium hydroxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1080/00958972.2020.1836359