2-(diacetoxyiodo)-1-[2-[(di-tert-butoxycarbonyl)amino]ethyl]-4,5-bis(ethoxymethoxy)benzene

Base Information

Chemical Name:2-(diacetoxyiodo)-1-[2-[(di-tert-butoxycarbonyl)amino]ethyl]-4,5-bis(ethoxymethoxy)benzene
CAS No.:1607804-00-1
Molecular Formula:C₂₈H₄₄INO₁₂
Molecular Weight:713.561
Hs Code.:

Synonyms:2-(diacetoxyiodo)-1-[2-[(di-tert-butoxycarbonyl)amino]ethyl]-4,5-bis(ethoxymethoxy)benzene

Suppliers and Price of 2-(diacetoxyiodo)-1-[2-[(di-tert-butoxycarbonyl)amino]ethyl]-4,5-bis(ethoxymethoxy)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of 2-(diacetoxyiodo)-1-[2-[(di-tert-butoxycarbonyl)amino]ethyl]-4,5-bis(ethoxymethoxy)benzene

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Technology Process of 2-(diacetoxyiodo)-1-[2-[(di-tert-butoxycarbonyl)amino]ethyl]-4,5-bis(ethoxymethoxy)benzene

There total 6 articles about 2-(diacetoxyiodo)-1-[2-[(di-tert-butoxycarbonyl)amino]ethyl]-4,5-bis(ethoxymethoxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2754-27-0
trimethylsilyl acetate

: 1607804-19-2
2-[2-[(di-tert-butoxycarbonyl)amino]ethyl]-4,5-bis(ethoxymethoxy)iodobenzene

: 1607804-00-1
2-(diacetoxyiodo)-1-[2-[(di-tert-butoxycarbonyl)amino]ethyl]-4,5-bis(ethoxymethoxy)benzene

Guidance literature:: With Selectfluor; In acetonitrile; at 20 ℃; for 5h; Inert atmosphere;

Reference yield:

: 1607804-24-9
N-t-butoxycarbonyl-2-(2-iodo-4,5-dihydroxyphenyl)ethanamine

: 1607804-00-1
2-(diacetoxyiodo)-1-[2-[(di-tert-butoxycarbonyl)amino]ethyl]-4,5-bis(ethoxymethoxy)benzene

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 18 h / 0 °C / Inert atmosphere; Reflux

2: triethylamine; dmap / acetonitrile / 24 h / 20 °C

3: Selectfluor / acetonitrile / 5 h / 20 °C / Inert atmosphere

With dmap; Selectfluor; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; acetonitrile;

Reference yield:

: 1607804-25-0
N-(t-butoxycarbonyl)-2-(2-iodo-4,5-bis(ethoxymethoxy)phenyl)ethanamine

: 1607804-00-1
2-(diacetoxyiodo)-1-[2-[(di-tert-butoxycarbonyl)amino]ethyl]-4,5-bis(ethoxymethoxy)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; dmap / acetonitrile / 24 h / 20 °C

2: Selectfluor / acetonitrile / 5 h / 20 °C / Inert atmosphere

With dmap; Selectfluor; triethylamine; In acetonitrile;