2′,3′,5′-tris-O-(tert-butyldimethylsilyl)-6-O-[2-(4-nitrophenyl)ethyl]guanosine

Base Information

Chemical Name:2′,3′,5′-tris-O-(tert-butyldimethylsilyl)-6-O-[2-(4-nitrophenyl)ethyl]guanosine
CAS No.:1203555-53-6
Molecular Formula:C₃₆H₆₂N₆O₇Si₃
Molecular Weight:775.181
Hs Code.:

Synonyms:2′,3′,5′-tris-O-(tert-butyldimethylsilyl)-6-O-[2-(4-nitrophenyl)ethyl]guanosine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2′,3′,5′-tris-O-(tert-butyldimethylsilyl)-6-O-[2-(4-nitrophenyl)ethyl]guanosine

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Technology Process of 2′,3′,5′-tris-O-(tert-butyldimethylsilyl)-6-O-[2-(4-nitrophenyl)ethyl]guanosine

There total 1 articles about 2′,3′,5′-tris-O-(tert-butyldimethylsilyl)-6-O-[2-(4-nitrophenyl)ethyl]guanosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 72409-24-6
2',3',5'-tri-O-(tert-butyldimethylsilyl)guanosine

: 100-27-6
2-(4-nitrophenyl)ethanol

: 1203555-53-6
2′,3′,5′-tris-O-(tert-butyldimethylsilyl)-6-O-[2-(4-nitrophenyl)ethyl]guanosine

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In 1,4-dioxane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1039/b909138f

Reference yield: 75.0%

: 1203555-53-6
2′,3′,5′-tris-O-(tert-butyldimethylsilyl)-6-O-[2-(4-nitrophenyl)ethyl]guanosine

: 2′,3′,5′-tris-O-(tert-butyldimethylsilyl)-6-O-[2-(4-nitrophenyl)ethyl]xanthosine

Guidance literature:: 2′,3′,5′-tris-O-(tert-butyldimethylsilyl)-6-O-[2-(4-nitrophenyl)ethyl]guanosine; With acetic acid; sodium nitrite; In water; acetone; at 0 ℃;

With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃;
DOI:10.1016/j.bmcl.2021.128439

Reference yield: 71.0%

: 1203555-53-6
2′,3′,5′-tris-O-(tert-butyldimethylsilyl)-6-O-[2-(4-nitrophenyl)ethyl]guanosine

: 1203555-54-7
2',3',5'-tris-O-(tert-butyldimethylsilyl)-O₆-[2-(4-nitrophenyl)-ethyl]-2-fluoro-inosine

Guidance literature:: With pyridine; tert.-butylnitrite; pyridine hydrogenfluoride; In tetrahydrofuran; at -25 ℃; for 0.116667h; Inert atmosphere;
DOI:10.1039/b909138f