2-bromo-4-<2-(trans-4-pentylcyclohexyl)ethyl>phenyl 4-<<(S)-6-methyloctyl>oxy>benzoate

Base Information

Chemical Name:2-bromo-4-<2-(trans-4-pentylcyclohexyl)ethyl>phenyl 4-<<(S)-6-methyloctyl>oxy>benzoate
CAS No.:115607-05-1
Molecular Formula:C₃₅H₅₁BrO₃
Molecular Weight:599.692
Hs Code.:

Synonyms:2-bromo-4-<2-(trans-4-pentylcyclohexyl)ethyl>phenyl 4-<<(S)-6-methyloctyl>oxy>benzoate

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Chemical Property of 2-bromo-4-<2-(trans-4-pentylcyclohexyl)ethyl>phenyl 4-<<(S)-6-methyloctyl>oxy>benzoate

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Technology Process of 2-bromo-4-<2-(trans-4-pentylcyclohexyl)ethyl>phenyl 4-<<(S)-6-methyloctyl>oxy>benzoate

There total 6 articles about 2-bromo-4-<2-(trans-4-pentylcyclohexyl)ethyl>phenyl 4-<<(S)-6-methyloctyl>oxy>benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1565-80-6
(2S)-2-methyl-1-butanol

: 115607-05-1
2-bromo-4-<2-(trans-4-pentylcyclohexyl)ethyl>phenyl 4-<<(S)-6-methyloctyl>oxy>benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 49.5 percent / Br₂, red P / 110 - 150 °C

2: 35 percent / Mg, Li₂CuCl₄ / tetrahydrofuran

3: 38 percent / KOH / ethanol; H₂O / Heating

4: N,N'- dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / CH₂Cl₂ / Ambient temperature

With dmap; phosphorus; potassium hydroxide; dilithium tetrachlorocuprate; bromine; magnesium; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1002/hlca.19880710218

Reference yield:

: 59177-09-2
(S)-1-bromo-6-methyloctane

: 115607-05-1
2-bromo-4-<2-(trans-4-pentylcyclohexyl)ethyl>phenyl 4-<<(S)-6-methyloctyl>oxy>benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 38 percent / KOH / ethanol; H₂O / Heating

2: N,N'- dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / CH₂Cl₂ / Ambient temperature

With dmap; potassium hydroxide; dicyclohexyl-carbodiimide; In ethanol; dichloromethane; water;
DOI:10.1002/hlca.19880710218

Reference yield:

: 534-00-9
(S)-2-methylbutyl bromide

: 115607-05-1
2-bromo-4-<2-(trans-4-pentylcyclohexyl)ethyl>phenyl 4-<<(S)-6-methyloctyl>oxy>benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 35 percent / Mg, Li₂CuCl₄ / tetrahydrofuran

2: 38 percent / KOH / ethanol; H₂O / Heating

3: N,N'- dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / CH₂Cl₂ / Ambient temperature

With dmap; potassium hydroxide; dilithium tetrachlorocuprate; magnesium; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1002/hlca.19880710218