(E)-O-3-p-tolylallyl benzylcarbamothioate

Base Information

Chemical Name:(E)-O-3-p-tolylallyl benzylcarbamothioate
CAS No.:1228453-85-7
Molecular Formula:C₁₈H₁₉NOS
Molecular Weight:297.421
Hs Code.:

Synonyms:(E)-O-3-p-tolylallyl benzylcarbamothioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-O-3-p-tolylallyl benzylcarbamothioate

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Technology Process of (E)-O-3-p-tolylallyl benzylcarbamothioate

There total 1 articles about (E)-O-3-p-tolylallyl benzylcarbamothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 122058-30-4
p-methylcinnamyl alcohol

: 622-78-6
Benzyl isothiocyanate

: 1228453-85-7
(E)-O-3-p-tolylallyl benzylcarbamothioate

Guidance literature:: p-methylcinnamyl alcohol; With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

Benzyl isothiocyanate; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo1006152

Reference yield: 35.0%

: 1228453-85-7
(E)-O-3-p-tolylallyl benzylcarbamothioate

: 1228453-97-1
C₁₈H₁₉NOS

: C₁₈H₁₉NOS

: C₁₈H₁₉NOS

Guidance literature:: With propylamine; O,O'-(S)-(1,1'-dinaphthyl-2,2'-diyl)-N,N-di-(S,S)-[2-phenylethylphosphoramidite]; bis(1,5-cyclooctadiene)diiridium(I) dichloride; potassium acetate; In 1,4-dioxane; at 50 ℃; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/jo1006152