(1S,2S,3R,5S)-pinanediol (1S)-(2-benzyloxy-1-p-methoxybenzyloxyethyl)boronate

Base Information

Chemical Name:(1S,2S,3R,5S)-pinanediol (1S)-(2-benzyloxy-1-p-methoxybenzyloxyethyl)boronate
CAS No.:1415693-06-9
Molecular Formula:C₂₇H₃₅BO₅
Molecular Weight:450.383
Hs Code.:

Synonyms:(1S,2S,3R,5S)-pinanediol (1S)-(2-benzyloxy-1-p-methoxybenzyloxyethyl)boronate

Suppliers and Price of (1S,2S,3R,5S)-pinanediol (1S)-(2-benzyloxy-1-p-methoxybenzyloxyethyl)boronate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2S,3R,5S)-pinanediol (1S)-(2-benzyloxy-1-p-methoxybenzyloxyethyl)boronate

Chemical Property:

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Technology Process of (1S,2S,3R,5S)-pinanediol (1S)-(2-benzyloxy-1-p-methoxybenzyloxyethyl)boronate

There total 5 articles about (1S,2S,3R,5S)-pinanediol (1S)-(2-benzyloxy-1-p-methoxybenzyloxyethyl)boronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 18680-27-8
pinanediol

: caesium (1S)-[2-benzyloxy-1-(p-methoxybenzyloxy)ethyl]trifluoroborate

: 1415693-06-9
(1S,2S,3R,5S)-pinanediol (1S)-(2-benzyloxy-1-p-methoxybenzyloxyethyl)boronate

Guidance literature:: With sodium hydrogencarbonate; In diethyl ether; water; at 22 ℃; Inert atmosphere;
DOI:10.1039/c2ob26756j

Reference yield:

: C₁₈H₂₅BO₃

: 1415693-06-9
(1S,2S,3R,5S)-pinanediol (1S)-(2-benzyloxy-1-p-methoxybenzyloxyethyl)boronate

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrahydrofuran / -100 °C

1.2: 15 h / -70 - 25 °C

2.1: tetrahydrofuran / -70 - 25 °C

3.1: cesium fluoride; caesium bifluoride; hydrogen fluoride / diethyl ether

4.1: sodium hydrogencarbonate / diethyl ether; water / 22 °C / Inert atmosphere

With caesium bifluoride; hydrogen fluoride; sodium hydrogencarbonate; cesium fluoride; In tetrahydrofuran; diethyl ether; water;
DOI:10.1039/c2ob26756j

Reference yield:

: 1415693-03-6
C₁₉H₂₆BClO₃

: 1415693-06-9
(1S,2S,3R,5S)-pinanediol (1S)-(2-benzyloxy-1-p-methoxybenzyloxyethyl)boronate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / -70 - 25 °C

2: cesium fluoride; caesium bifluoride; hydrogen fluoride / diethyl ether

3: sodium hydrogencarbonate / diethyl ether; water / 22 °C / Inert atmosphere

With caesium bifluoride; hydrogen fluoride; sodium hydrogencarbonate; cesium fluoride; In tetrahydrofuran; diethyl ether; water;
DOI:10.1039/c2ob26756j