3-methyl-1-[10-(methanesulfinyl)decan-1-yl]-1H-imidazolium p-toluenesulfonate

Base Information

Chemical Name:3-methyl-1-[10-(methanesulfinyl)decan-1-yl]-1H-imidazolium p-toluenesulfonate
CAS No.:1393662-15-1
Molecular Formula:C₇H₇O₃S*C₁₅H₂₉N₂OS
Molecular Weight:456.671
Hs Code.:

Synonyms:3-methyl-1-[10-(methanesulfinyl)decan-1-yl]-1H-imidazolium p-toluenesulfonate

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Chemical Property of 3-methyl-1-[10-(methanesulfinyl)decan-1-yl]-1H-imidazolium p-toluenesulfonate

Chemical Property:

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Technology Process of 3-methyl-1-[10-(methanesulfinyl)decan-1-yl]-1H-imidazolium p-toluenesulfonate

There total 5 articles about 3-methyl-1-[10-(methanesulfinyl)decan-1-yl]-1H-imidazolium p-toluenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1393662-11-7
3-methyl-1-[10-(methylthio)decan-1-yl]-1H-imidazolium p-toluenesulfonate

: 1393662-15-1
3-methyl-1-[10-(methanesulfinyl)decan-1-yl]-1H-imidazolium p-toluenesulfonate

Guidance literature:: With dihydrogen peroxide; In methanol; water; at 0 - 20 ℃; for 2h;
DOI:10.1016/j.tet.2012.06.026

Reference yield:

: 855753-25-2
10-(methylthio)decan-1-ol

: 1393662-15-1
3-methyl-1-[10-(methanesulfinyl)decan-1-yl]-1H-imidazolium p-toluenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: trimethylamine hydrochloride; triethylamine / dichloromethane / 1 h / 0 °C

2: acetonitrile / 48 h / 60 °C

3: dihydrogen peroxide / methanol; water / 2 h / 0 - 20 °C

With dihydrogen peroxide; trimethylamine hydrochloride; triethylamine; In methanol; dichloromethane; water; acetonitrile;
DOI:10.1016/j.tet.2012.06.026

Reference yield:

: 53463-68-6
1-bromo-10-decanol

: 1393662-15-1
3-methyl-1-[10-(methanesulfinyl)decan-1-yl]-1H-imidazolium p-toluenesulfonate

Guidance literature:: Multi-step reaction with 5 steps

1.1: thiourea; potassium iodide / ethanol / 14 h / Reflux

1.2: 3 h / Reflux

1.3: 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 0 - 20 °C

3.1: trimethylamine hydrochloride; triethylamine / dichloromethane / 1 h / 0 °C

4.1: acetonitrile / 48 h / 60 °C

5.1: dihydrogen peroxide / methanol; water / 2 h / 0 - 20 °C

With dihydrogen peroxide; trimethylamine hydrochloride; potassium carbonate; triethylamine; thiourea; potassium iodide; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2012.06.026