1-methyl-3-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1H-imidazol-3-ium hexafluorophosphate

Base Information

Chemical Name:1-methyl-3-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1H-imidazol-3-ium hexafluorophosphate
CAS No.:1393092-13-1
Molecular Formula:C₁₄H₁₆N₅*F₆P
Molecular Weight:399.279
Hs Code.:

Synonyms:1-methyl-3-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1H-imidazol-3-ium hexafluorophosphate

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Chemical Property of 1-methyl-3-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1H-imidazol-3-ium hexafluorophosphate

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Technology Process of 1-methyl-3-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1H-imidazol-3-ium hexafluorophosphate

There total 3 articles about 1-methyl-3-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1H-imidazol-3-ium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1392270-70-0
1-((1-benzyl)-1H-1,2,3-triazol-4-yl)methyl-3-methyl-1H-imidazolium bromide

: 1393092-13-1
1-methyl-3-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1H-imidazol-3-ium hexafluorophosphate

Guidance literature:: With ammonium hexafluorophosphate; In methanol; for 24h;
DOI:10.1002/cmdc.202100311

Reference yield:

: 813458-72-9
1-methyl-3-(prop-2-yn-1-yl)-1H-imidazol-3-ium bromide

: 1393092-13-1
1-methyl-3-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1H-imidazol-3-ium hexafluorophosphate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium azide / methanol; water / 2 h / Reflux

1.2: 24 h / 20 °C

2.1: potassium hexafluorophosphate / water; acetone / 12 h / 25 °C

With potassium hexafluorophosphate; sodium azide; In methanol; water; acetone;
DOI:10.1002/chem.201103631

Reference yield:

: 813458-72-9
1-methyl-3-(prop-2-yn-1-yl)-1H-imidazol-3-ium bromide

: 622-79-7
benzyl azide

: 1393092-13-1
1-methyl-3-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1H-imidazol-3-ium hexafluorophosphate

Guidance literature:: Multi-step reaction with 2 steps

1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / tetrahydrofuran; water / 24 h / 20 °C / Schlenk technique; Inert atmosphere

2: ammonium hexafluorophosphate / methanol / 24 h

With copper(ll) sulfate pentahydrate; ammonium hexafluorophosphate; sodium L-ascorbate; In tetrahydrofuran; methanol; water;
DOI:10.1002/cmdc.202100311