(E)-3-(2'-formyl-3'-hydroxyphenyl)ethenoic acid

Base Information

Chemical Name:(E)-3-(2'-formyl-3'-hydroxyphenyl)ethenoic acid
CAS No.:1628227-04-2
Molecular Formula:C₁₀H₈O₄
Molecular Weight:192.171
Hs Code.:

Synonyms:(E)-3-(2'-formyl-3'-hydroxyphenyl)ethenoic acid

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Chemical Property of (E)-3-(2'-formyl-3'-hydroxyphenyl)ethenoic acid

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Technology Process of (E)-3-(2'-formyl-3'-hydroxyphenyl)ethenoic acid

There total 2 articles about (E)-3-(2'-formyl-3'-hydroxyphenyl)ethenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1628227-03-1
ethyl (E)-3-(2'-formyl-3'-hydroxyphenyl)ethenoate

: 1628227-04-2
(E)-3-(2'-formyl-3'-hydroxyphenyl)ethenoic acid

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; water; at 0 ℃; for 5h; Reagent/catalyst;
DOI:10.1515/hc-2014-0053

Reference yield:

: 524705-75-7
(E)-5-(2'-ethoxycarbonyl)ethenyl-2,2-dimethyl-4H-benzo[e][1,3]dioxine

: 1628227-04-2
(E)-3-(2'-formyl-3'-hydroxyphenyl)ethenoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / water; tetrahydrofuran / 72 h / 20 °C

2: manganese(IV) oxide / dimethyl sulfoxide; chloroform / 5 h / 20 °C

3: lithium hydroxide / water; tetrahydrofuran / 5 h / 0 °C

With manganese(IV) oxide; toluene-4-sulfonic acid; lithium hydroxide; In tetrahydrofuran; chloroform; water; dimethyl sulfoxide;
DOI:10.1515/hc-2014-0053