(S,Z)-N-((1-benzyl-1H-indol-2-yl)methylene)-4-methyl benzenesulfinimide

Base Information

Chemical Name:(S,Z)-N-((1-benzyl-1H-indol-2-yl)methylene)-4-methyl benzenesulfinimide
CAS No.:1424168-08-0
Molecular Formula:C₂₃H₂₀N₂OS
Molecular Weight:372.491
Hs Code.:

Synonyms:(S,Z)-N-((1-benzyl-1H-indol-2-yl)methylene)-4-methyl benzenesulfinimide

Suppliers and Price of (S,Z)-N-((1-benzyl-1H-indol-2-yl)methylene)-4-methyl benzenesulfinimide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S,Z)-N-((1-benzyl-1H-indol-2-yl)methylene)-4-methyl benzenesulfinimide

Chemical Property:

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Technology Process of (S,Z)-N-((1-benzyl-1H-indol-2-yl)methylene)-4-methyl benzenesulfinimide

There total 5 articles about (S,Z)-N-((1-benzyl-1H-indol-2-yl)methylene)-4-methyl benzenesulfinimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 81787-94-2
1-benzylindole-2-carbaldehyde

: 188447-91-8
(S)-p-toluenesulfinimide

: 1424168-08-0
(S,Z)-N-((1-benzyl-1H-indol-2-yl)methylene)-4-methyl benzenesulfinimide

Guidance literature:: With titanium(IV) isopropylate; In dichloromethane; for 5h; Reflux;
DOI:10.1002/cjoc.201200672

Reference yield:

: 187264-03-5
(1-benzyl-1H-indol-2-yl)methanol

: 1424168-08-0
(S,Z)-N-((1-benzyl-1H-indol-2-yl)methylene)-4-methyl benzenesulfinimide

Guidance literature:: Multi-step reaction with 2 steps

1: manganese(IV) oxide / dichloromethane / 32 h / 20 °C

2: titanium(IV) isopropylate / dichloromethane / 5 h / Reflux

With titanium(IV) isopropylate; manganese(IV) oxide; In dichloromethane;
DOI:10.1002/cjoc.201200672

Reference yield:

Indole-2-carboxylic acid: 1477-50-5,1228050-17-6
Indole-2-carboxylic acid

: 1424168-08-0
(S,Z)-N-((1-benzyl-1H-indol-2-yl)methylene)-4-methyl benzenesulfinimide

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuryl dichloride / 2 h / 0 °C / Reflux

2.1: potassium hydroxide / dimethyl sulfoxide / 0.5 h

2.2: 1 h

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

4.1: manganese(IV) oxide / dichloromethane / 32 h / 20 °C

5.1: titanium(IV) isopropylate / dichloromethane / 5 h / Reflux

With titanium(IV) isopropylate; manganese(IV) oxide; lithium aluminium tetrahydride; sulfuryl dichloride; potassium hydroxide; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide;
DOI:10.1002/cjoc.201200672