1,4-Dimesityl-3-ol-1,2,4-butantrion

Base Information

• Chemical Name: 1,4-Dimesityl-3-ol-1,2,4-butantrion
• CAS No.: 130992-62-0
• Molecular Formula: C₂₂H₂₄O₄
• Molecular Weight: 352.43

Synonyms:1,4-Dimesityl-3-ol-1,2,4-butantrion

Chemical Property of 1,4-Dimesityl-3-ol-1,2,4-butantrion

Chemical Property:

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Technology Process of 1,4-Dimesityl-3-ol-1,2,4-butantrion

There total 1 articles about 1,4-Dimesityl-3-ol-1,2,4-butantrion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

mesitylglyoxal (22185-97-3) → 1,4-Dimesityl-3-ol-1,2,4-butantrion (130992-62-0)

Guidance literature:

potassium cyanide; In ethanol;

Reference yield: 90.0%

1,4-Dimesityl-3-ol-1,2,4-butantrion (130992-62-0) → dimesityl-butanetetraone (19909-65-0)

Guidance literature:

With nitric acid; at 60 ℃;

Reference yield:

1,4-Dimesityl-3-ol-1,2,4-butantrion (130992-62-0) → C22H22O4(1-)*Cs(1+)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / HNO₃ conc. / 60 °C

2: Cs / tetrahydrofuran

With o-chlorobenzylidene malononitrile; nitric acid; In tetrahydrofuran;

upstream raw materials:

mesitylglyoxal

Downstream raw materials:

dimesityl-butanetetraone

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