2-exo,3-exo,5-exo,6-exo-tetrakis(chloromethyl)-7-(diphenylmethylidene)bicyclo<2.2.1>heptane

Base Information

Chemical Name:2-exo,3-exo,5-exo,6-exo-tetrakis(chloromethyl)-7-(diphenylmethylidene)bicyclo<2.2.1>heptane
CAS No.:120567-53-5
Molecular Formula:C₂₄H₂₄Cl₄
Molecular Weight:454.267
Hs Code.:

Synonyms:2-exo,3-exo,5-exo,6-exo-tetrakis(chloromethyl)-7-(diphenylmethylidene)bicyclo<2.2.1>heptane

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Chemical Property of 2-exo,3-exo,5-exo,6-exo-tetrakis(chloromethyl)-7-(diphenylmethylidene)bicyclo<2.2.1>heptane

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Technology Process of 2-exo,3-exo,5-exo,6-exo-tetrakis(chloromethyl)-7-(diphenylmethylidene)bicyclo<2.2.1>heptane

There total 3 articles about 2-exo,3-exo,5-exo,6-exo-tetrakis(chloromethyl)-7-(diphenylmethylidene)bicyclo<2.2.1>heptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 120567-52-4
7-(diphenylmethylidene)bicyclo<2.2.1>heptane-2-exo,3-exo,5-exo,6-exo-tetramethanol

: 120567-53-5
2-exo,3-exo,5-exo,6-exo-tetrakis(chloromethyl)-7-(diphenylmethylidene)bicyclo<2.2.1>heptane

Guidance literature:: With pyridine; thionyl chloride; at 60 ℃; for 3h;
DOI:10.1002/hlca.19880710538

Reference yield:

: 4502-48-1
<2.2.1>bicyclo-5-heptene-7-diphenylmethylene-2,3-exo-dicarboxylic anhydride

: 120567-53-5
2-exo,3-exo,5-exo,6-exo-tetrakis(chloromethyl)-7-(diphenylmethylidene)bicyclo<2.2.1>heptane

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / 10percent Pd/C / 60 h / 20 °C / 2280 Torr

2: 73 percent / LiAlH₄ / tetrahydrofuran / Heating

3: 50 percent / SOCl₂, pyridine / 3 h / 60 °C

With pyridine; lithium aluminium tetrahydride; thionyl chloride; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1002/hlca.19880710538

Reference yield:

: 120567-51-3
tetramethyl 7-(diphenylmethylidene)bicyclo<2.2.1>heptane-2-exo,3-exo,5-exo,6-exo-tetracarboxylate

: 120567-53-5
2-exo,3-exo,5-exo,6-exo-tetrakis(chloromethyl)-7-(diphenylmethylidene)bicyclo<2.2.1>heptane

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / LiAlH₄ / tetrahydrofuran / Heating

2: 50 percent / SOCl₂, pyridine / 3 h / 60 °C

With pyridine; lithium aluminium tetrahydride; thionyl chloride; In tetrahydrofuran;
DOI:10.1002/hlca.19880710538