(2R,3R)-2,3-bis((tert-butyldiphenylsiloxy)methyl)-1,1-bis(methylthio)cyclobutane

Base Information

Chemical Name:(2R,3R)-2,3-bis((tert-butyldiphenylsiloxy)methyl)-1,1-bis(methylthio)cyclobutane
CAS No.:129215-08-3
Molecular Formula:C₄₀H₅₂O₂S₂Si₂
Molecular Weight:685.155
Hs Code.:

Synonyms:(2R,3R)-2,3-bis((tert-butyldiphenylsiloxy)methyl)-1,1-bis(methylthio)cyclobutane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3R)-2,3-bis((tert-butyldiphenylsiloxy)methyl)-1,1-bis(methylthio)cyclobutane

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Technology Process of (2R,3R)-2,3-bis((tert-butyldiphenylsiloxy)methyl)-1,1-bis(methylthio)cyclobutane

There total 4 articles about (2R,3R)-2,3-bis((tert-butyldiphenylsiloxy)methyl)-1,1-bis(methylthio)cyclobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 124282-17-3
(1R,2R)-(3,3-bis(methylthio)-2-(hydroxymethyl)cyclobutyl)methanol

: 58479-61-1
tert-butylchlorodiphenylsilane

: 129215-08-3
(2R,3R)-2,3-bis((tert-butyldiphenylsiloxy)methyl)-1,1-bis(methylthio)cyclobutane

Guidance literature:: With 1H-imidazole; dmap; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1021/ja00049a020

Reference yield: 100.0%

: 129215-08-3
(2R,3R)-2,3-bis((tert-butyldiphenylsiloxy)methyl)-1,1-bis(methylthio)cyclobutane

Guidance literature:

Reference yield:

: 124282-19-5
methyl (1R,2R)-3,3-bis(methylthio)-2-((2-oxo-1,3-oxazolidin-3-yl)carbonyl)cyclobutanecarboxylate

: 129215-08-3
(2R,3R)-2,3-bis((tert-butyldiphenylsiloxy)methyl)-1,1-bis(methylthio)cyclobutane

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / tetrahydrofuran; CCl₄ / 0.17 h / 0 °C

2: 97 percent / lithium aluminum hydride / tetrahydrofuran / 0.17 h / 0 °C

3: 100 percent / imidazole, 4-(dimethylamino)pyridine (DMAP) / dimethylformamide / Ambient temperature

With 1H-imidazole; dmap; lithium aluminium tetrahydride; In tetrahydrofuran; tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00049a020