Technology Process of 28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,2',3',4',6'-hepta-O-benzoyl-β-D-gentiopyranoside
There total 1 articles about 28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,2',3',4',6'-hepta-O-benzoyl-β-D-gentiopyranoside which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate; C63H50Cl3NO16;
In
dichloromethane;
at 20 ℃;
for 0.5h;
Molecular sieve;
With
trimethylsilyl trifluoromethanesulfonate;
In
dichloromethane;
at -30 - 20 ℃;
for 1.5h;
Molecular sieve;
DOI:10.1016/j.ejmech.2014.03.080
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
methanol; dichloromethane;
for 5h;
under 760.051 Torr;
DOI:10.1016/j.ejmech.2014.03.080
