28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,2',3',4',6'-hepta-O-benzoyl-β-D-gentiopyranoside

Base Information

Chemical Name:28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,2',3',4',6'-hepta-O-benzoyl-β-D-gentiopyranoside
CAS No.:1609983-99-4
Molecular Formula:C₁₃₃H₁₂₉NO₃₀
Molecular Weight:2221.48
Hs Code.:

Synonyms:28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,2',3',4',6'-hepta-O-benzoyl-β-D-gentiopyranoside

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Chemical Property of 28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,2',3',4',6'-hepta-O-benzoyl-β-D-gentiopyranoside

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Technology Process of 28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,2',3',4',6'-hepta-O-benzoyl-β-D-gentiopyranoside

There total 1 articles about 28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,2',3',4',6'-hepta-O-benzoyl-β-D-gentiopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1609983-87-0
6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate

: C₆₃H₅₀Cl₃NO₁₆

: 1609983-99-4
28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,2',3',4',6'-hepta-O-benzoyl-β-D-gentiopyranoside

Guidance literature:: 6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate; C₆₃H₅₀Cl₃NO₁₆; In dichloromethane; at 20 ℃; for 0.5h; Molecular sieve;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -30 - 20 ℃; for 1.5h; Molecular sieve;
DOI:10.1016/j.ejmech.2014.03.080

Reference yield:

: 1609983-99-4
28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,2',3',4',6'-hepta-O-benzoyl-β-D-gentiopyranoside

: C₁₂₆H₁₂₃NO₃₀

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; dichloromethane; for 5h; under 760.051 Torr;
DOI:10.1016/j.ejmech.2014.03.080