α-<2-(3,4-dimethoxyphenyl)-1-methyl-1H-imidazol-4-yl>-4-morpholineacetonitrile

Base Information

Chemical Name:α-<2-(3,4-dimethoxyphenyl)-1-methyl-1H-imidazol-4-yl>-4-morpholineacetonitrile
CAS No.:99280-86-1
Molecular Formula:C₁₈H₂₂N₄O₃
Molecular Weight:342.398
Hs Code.:

Synonyms:α-<2-(3,4-dimethoxyphenyl)-1-methyl-1H-imidazol-4-yl>-4-morpholineacetonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-<2-(3,4-dimethoxyphenyl)-1-methyl-1H-imidazol-4-yl>-4-morpholineacetonitrile

Chemical Property:

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Technology Process of α-<2-(3,4-dimethoxyphenyl)-1-methyl-1H-imidazol-4-yl>-4-morpholineacetonitrile

There total 5 articles about α-<2-(3,4-dimethoxyphenyl)-1-methyl-1H-imidazol-4-yl>-4-morpholineacetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2024-83-1
veratronitrile

: 99280-86-1
α-<2-(3,4-dimethoxyphenyl)-1-methyl-1H-imidazol-4-yl>-4-morpholineacetonitrile

Guidance literature:: Multi-step reaction with 5 steps

1: 61 percent / HCl gas / 23 °C

2: 76 percent / NH₃ / 4 h / 68 °C / 21720.2 Torr

3: MnO₂ / tetrahydrofuran / 1.5 h / Heating

4: sodium methoxide / dimethylformamide / 6 h / 23 °C

5: p-toluenesulfonic acid monohydrate / dioxane / 1.5 h / Heating

With hydrogenchloride; manganese(IV) oxide; ammonia; sodium methylate; toluene-4-sulfonic acid; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1021/jm00152a015

Reference yield:

: 53292-69-6
2-(3,4-dimethoxyphenyl)-1H-imidazole-4-methanol

: 99280-86-1
α-<2-(3,4-dimethoxyphenyl)-1-methyl-1H-imidazol-4-yl>-4-morpholineacetonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: MnO₂ / tetrahydrofuran / 1.5 h / Heating

2: sodium methoxide / dimethylformamide / 6 h / 23 °C

3: p-toluenesulfonic acid monohydrate / dioxane / 1.5 h / Heating

With manganese(IV) oxide; sodium methylate; toluene-4-sulfonic acid; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1021/jm00152a015

Reference yield:

: 99280-82-7
2-(3,4-Dimethoxy-phenyl)-1H-imidazole-4-carbaldehyde

: 99280-86-1
α-<2-(3,4-dimethoxyphenyl)-1-methyl-1H-imidazol-4-yl>-4-morpholineacetonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methoxide / dimethylformamide / 6 h / 23 °C

2: p-toluenesulfonic acid monohydrate / dioxane / 1.5 h / Heating

With sodium methylate; toluene-4-sulfonic acid; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1021/jm00152a015