cis-{1,3-bis(diphenylphosphino)dicyclopentadiene}(tetracarbonyl)molybdenum

Base Information

Chemical Name:cis-{1,3-bis(diphenylphosphino)dicyclopentadiene}(tetracarbonyl)molybdenum
CAS No.:115530-00-2
Molecular Formula:C₃₈H₃₀MoO₄P₂
Molecular Weight:708.541
Hs Code.:

Synonyms:cis-{1,3-bis(diphenylphosphino)dicyclopentadiene}(tetracarbonyl)molybdenum

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Chemical Property of cis-{1,3-bis(diphenylphosphino)dicyclopentadiene}(tetracarbonyl)molybdenum

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Technology Process of cis-{1,3-bis(diphenylphosphino)dicyclopentadiene}(tetracarbonyl)molybdenum

There total 7 articles about cis-{1,3-bis(diphenylphosphino)dicyclopentadiene}(tetracarbonyl)molybdenum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: C₇H₈Mo(CO)4

: 115530-00-2
cis-{1,3-bis(diphenylphosphino)dicyclopentadiene}(tetracarbonyl)molybdenum

Guidance literature:: With (diphenylphosphino)cyclopentadiene; In hexane; under N2 or vac.; soln. of Mo-complex in hexane added dropwise to a freshly prepd. soln. of the P-compd. in hexane at room temp., stirred 3h at room temp., white pptn.; filtered, recrystn. (toluene-hexane = 1:1), dried (vac.), elem. anal.;
DOI:10.1016/S0277-5387(00)86780-7

Reference yield: 85.0%

: 23581-79-5,37834-17-6,42724-61-8
cis-Mo(CO)4(Ph₂PCl)2

: cyclopentadienylthallium(I)

: 115530-00-2
cis-{1,3-bis(diphenylphosphino)dicyclopentadiene}(tetracarbonyl)molybdenum

Guidance literature:: In toluene; under N2 or vac.; soln. of Mo-complex in toluene added dropwise to a suspn. of Tl-compd. in toluene at room temp., refluxed overnight; cooled to room temp., filtered, concd. (vac.), n-hexane added until soln. turned cloudy, crystn. at room temp. overnight;
DOI:10.1016/S0277-5387(00)86780-7