methyl 5(S)-amino-7-methyl-2(R)-(phenylmethyl)-3-trans-octenoate trifluoroacetate

Base Information

Chemical Name:methyl 5(S)-amino-7-methyl-2(R)-(phenylmethyl)-3-trans-octenoate trifluoroacetate
CAS No.:109065-06-7
Molecular Formula:C₂HF₃O₂*C₁₇H₂₅NO₂
Molecular Weight:389.415
Hs Code.:

Synonyms:methyl 5(S)-amino-7-methyl-2(R)-(phenylmethyl)-3-trans-octenoate trifluoroacetate

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Chemical Property of methyl 5(S)-amino-7-methyl-2(R)-(phenylmethyl)-3-trans-octenoate trifluoroacetate

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Technology Process of methyl 5(S)-amino-7-methyl-2(R)-(phenylmethyl)-3-trans-octenoate trifluoroacetate

There total 2 articles about methyl 5(S)-amino-7-methyl-2(R)-(phenylmethyl)-3-trans-octenoate trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.7%

: 109065-04-5
methyl 5(S)--7-methyl-2(R)-(phenylmethyl)-3-trans-octenoate

: 76-05-1
trifluoroacetic acid

: 109065-06-7
methyl 5(S)-amino-7-methyl-2(R)-(phenylmethyl)-3-trans-octenoate trifluoroacetate

Guidance literature:: In dichloromethane; for 0.166667h; Ambient temperature;
DOI:10.1021/jm00392a016

Reference yield:

: 109065-03-4
5(S)--7-methyl-2(R)-(phenylmethyl)-3-trans-octenoic acid

: 109065-06-7
methyl 5(S)-amino-7-methyl-2(R)-(phenylmethyl)-3-trans-octenoate trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 99.5 percent / diethyl ether / 0 °C

2: 93.7 percent / CH₂Cl₂ / 0.17 h / Ambient temperature

In diethyl ether; dichloromethane;
DOI:10.1021/jm00392a016

Reference yield: 78.1%

: 108385-36-0
4(S)-<(tert-butyloxycarbonyl)amino>-2,2-difluoro-3(R)-hydroxy-5-isopropylpentanoic aicd

: 109065-06-7
methyl 5(S)-amino-7-methyl-2(R)-(phenylmethyl)-3-trans-octenoate trifluoroacetate

: 109065-07-8
methyl 5(S)-<<4(S)--2,2-difluoro-3(R)-hydroxy-6-methylheptanoyl>amino>-7-methyl-2(R)-(phenylmethyl)-3-trans-octenoate

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1021/jm00392a016