(2'E)-1-(3,7,11,15-tetramethylhexadec-2-enyl)-6-methyl-2,3,4,5-tetramethoxybenzene

Base Information

Chemical Name:(2'E)-1-(3,7,11,15-tetramethylhexadec-2-enyl)-6-methyl-2,3,4,5-tetramethoxybenzene
CAS No.:109364-39-8
Molecular Formula:C₃₁H₅₄O₄
Molecular Weight:490.767
Hs Code.:

Synonyms:(2'E)-1-(3,7,11,15-tetramethylhexadec-2-enyl)-6-methyl-2,3,4,5-tetramethoxybenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2'E)-1-(3,7,11,15-tetramethylhexadec-2-enyl)-6-methyl-2,3,4,5-tetramethoxybenzene

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Technology Process of (2'E)-1-(3,7,11,15-tetramethylhexadec-2-enyl)-6-methyl-2,3,4,5-tetramethoxybenzene

There total 2 articles about (2'E)-1-(3,7,11,15-tetramethylhexadec-2-enyl)-6-methyl-2,3,4,5-tetramethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106-44-5
p-cresol

: 109364-39-8
(2'E)-1-(3,7,11,15-tetramethylhexadec-2-enyl)-6-methyl-2,3,4,5-tetramethoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / iron powder, bromine / CHCl₃ / 48 h / Ambient temperature

2: 1.) NaOMe, CuCN / 1.) methanol, DME, dimethyl carbonate, 80 deg C, 5 h 2.) methanol, DME, water, RT, 2 h

With bromine; sodium methylate; iron; In chloroform;
DOI:10.1021/jo00226a028

Reference yield:

: 35896-58-3
2,3,4,5-tetramethoxytoluene

: 943232-38-0
(7R,11R)-3,7,11,15-tetramethyl-2-hexadecenyl bromide

: 109364-39-8
(2'E)-1-(3,7,11,15-tetramethylhexadec-2-enyl)-6-methyl-2,3,4,5-tetramethoxybenzene

Guidance literature:: Yield given. Multistep reaction;
DOI:10.1021/jo00226a028

Reference yield: 84.0%

: 109364-39-8
(2'E)-1-(3,7,11,15-tetramethylhexadec-2-enyl)-6-methyl-2,3,4,5-tetramethoxybenzene

: 51077-59-9,7690-75-7
(2'E)-2-(3,7,11,15-tetramethylhexadec-2-enyl)-3-methyl-5,6-dimethoxy-1,4-benzoquinone

Guidance literature:: With Pyridine-2,6-dicarboxylic acid; ammonium cerium(IV) nitrate; In water; acetonitrile; a.) 20 min, 0 deg C b.) 10 min, RT;
DOI:10.1021/jo00226a028