C₅₄H₇₂N₂O₁₂SSi

Base Information

• Chemical Name: C₅₄H₇₂N₂O₁₂SSi
• CAS No.: 1316758-54-9
• Molecular Formula: C₅₄H₇₂N₂O₁₂SSi
• Molecular Weight: 1001.32
• Mol file: 1316758-54-9.mol

Synonyms:C₅₄H₇₂N₂O₁₂SSi

Chemical Property of C₅₄H₇₂N₂O₁₂SSi

Chemical Property:

Purity/Quality:

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• Pictogram(s):  
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MSDS Files:

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Technology Process of C₅₄H₇₂N₂O₁₂SSi

There total 3 articles about C₅₄H₇₂N₂O₁₂SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

C50H66N2O10SSi (1316758-53-8) + methyl (S)-2-[(trifluoromethanesulfonyl)oxy]propionate (99208-98-7) → C54H72N2O12SSi (1316758-54-9)

Guidance literature:

C₅₀H₆₆N₂O₁₀SSi; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.166667h;

methyl (S)-2-[(trifluoromethanesulfonyl)oxy]propionate; In tetrahydrofuran; mineral oil; at 0 ℃; for 2h;

DOI:10.1021/ol201806d

Reference yield:

C64H67ClN2O13SSi (1316758-49-2) → C54H72N2O12SSi (1316758-54-9)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium tetrahydroborate / tetrahydrofuran; 2-methyl-propan-1-ol; water / 0 - 20 °C

2.1: acetic acid / tetrahydrofuran; 2-methyl-propan-1-ol; water / 0 °C / Heating

2.2: 0.5 h / 20 °C

2.3: 3 h

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 0 °C

3.2: 2 h / 0 °C

With sodium tetrahydroborate; sodium hydride; acetic acid; In tetrahydrofuran; 2-methyl-propan-1-ol; water; mineral oil;

DOI:10.1021/ol201806d

Reference yield:

C48H63ClN2O9SSi → C54H72N2O12SSi (1316758-54-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: acetic acid / tetrahydrofuran; 2-methyl-propan-1-ol; water / 0 °C / Heating

1.2: 0.5 h / 20 °C

1.3: 3 h

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 0 °C

2.2: 2 h / 0 °C

With sodium hydride; acetic acid; In tetrahydrofuran; 2-methyl-propan-1-ol; water; mineral oil;

DOI:10.1021/ol201806d

upstream raw materials:

C₆₄H₆₇ClN₂O₁₃SSi

C₅₀H₆₆N₂O₁₀SSi

methyl (S)-2-[(trifluoromethanesulfonyl)oxy]propionate

Downstream raw materials:

C₆₁H₇₉N₂O₁₆PSi