3-[2-(4-methoxy-phenyl)-cyclopropyl]-2-methyl-1,1-bis-methylsulfanyl-hexa-1,5-dien-3-ol

Base Information

• Chemical Name: 3-[2-(4-methoxy-phenyl)-cyclopropyl]-2-methyl-1,1-bis-methylsulfanyl-hexa-1,5-dien-3-ol
• CAS No.: 1027940-54-0
• Molecular Formula: C₁₉H₂₆O₂S₂
• Molecular Weight: 350.546

Synonyms:3-[2-(4-methoxy-phenyl)-cyclopropyl]-2-methyl-1,1-bis-methylsulfanyl-hexa-1,5-dien-3-ol

Chemical Property of 3-[2-(4-methoxy-phenyl)-cyclopropyl]-2-methyl-1,1-bis-methylsulfanyl-hexa-1,5-dien-3-ol

Chemical Property:

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Technology Process of 3-[2-(4-methoxy-phenyl)-cyclopropyl]-2-methyl-1,1-bis-methylsulfanyl-hexa-1,5-dien-3-ol

There total 1 articles about 3-[2-(4-methoxy-phenyl)-cyclopropyl]-2-methyl-1,1-bis-methylsulfanyl-hexa-1,5-dien-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-<2-bis(methylthio)methylenepropanoyl>-2-(4-methoxyphenyl)cyclopropane (132610-23-2) → 3-[2-(4-methoxy-phenyl)-cyclopropyl]-2-methyl-1,1-bis-methylsulfanyl-hexa-1,5-dien-3-ol (1027940-54-0)

Guidance literature:

CH₂=CHCH₂X; With magnesium; In diethyl ether; at 20 ℃; for 1h;

1-<2-bis(methylthio)methylenepropanoyl>-2-(4-methoxyphenyl)cyclopropane; In tetrahydrofuran; diethyl ether; at 20 ℃; for 3h; Further stages.;

DOI:10.1021/jo001488p

Reference yield: 67.0%

3-[2-(4-methoxy-phenyl)-cyclopropyl]-2-methyl-1,1-bis-methylsulfanyl-hexa-1,5-dien-3-ol (1027940-54-0) → S-methyl 2-(prop-1-ene-3-yl)-5-(4-methoxyphenyl)-1-methylcyclopent-2-en-1-carbothioate

Guidance literature:

With boron trifluoride diethyl etherate; In nitromethane; at 0 - 20 ℃;

DOI:10.1021/jo001488p

Reference yield:

3-[2-(4-methoxy-phenyl)-cyclopropyl]-2-methyl-1,1-bis-methylsulfanyl-hexa-1,5-dien-3-ol (1027940-54-0) → 1-(4-methoxyphenyl)-4-methyl-5-(methylthio)indane

Guidance literature:

With boron trifluoride diethyl etherate; In benzene; for 5h; Heating;

DOI:10.1021/jo001488p

upstream raw materials:

1-<2-bis(methylthio)methylenepropanoyl>-2-(4-methoxyphenyl)cyclopropane

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