1-(2,6-dimethylphenyl)-1H-pyrazole

Base Information

Chemical Name:1-(2,6-dimethylphenyl)-1H-pyrazole
CAS No.:38581-14-5
Molecular Formula:C₁₁H₁₂N₂
Molecular Weight:172.23
Hs Code.:

Synonyms:1-(2,6-dimethylphenyl)-1H-pyrazole

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Chemical Property of 1-(2,6-dimethylphenyl)-1H-pyrazole

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Technology Process of 1-(2,6-dimethylphenyl)-1H-pyrazole

There total 5 articles about 1-(2,6-dimethylphenyl)-1H-pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 288-13-1
NH-pyrazole

: 443-88-9
2-fluoro-m-xylene

: 38581-14-5
1-(2,6-dimethylphenyl)-1H-pyrazole

Guidance literature:: With 3,6‐di‐tert‐butyl‐9‐(4‐fluoro‐2,6‐dimethylphenyl)xanthylium tetrafluoroborate; at 45 - 50 ℃; for 18h; Irradiation; Inert atmosphere; Sealed tube;
DOI:10.1021/jacs.0c09296

Reference yield:

: 823-96-1
Trimethylboroxine

: 1126-00-7
1-phenylpyrazole

: 20157-44-2
1-o-tolyl-1H-pyrazole

: 38581-14-5
1-(2,6-dimethylphenyl)-1H-pyrazole

Guidance literature:: With pentamethylcyclopentadienyl(benzene)cobalt(III) hexafluorophosphate; potassium carbonate; silver carbonate; In 2-methyltetrahydrofuran; at 60 ℃; for 16h; Overall yield = 86 percent; Inert atmosphere; Sealed tube;
DOI:10.1038/s41557-020-0475-7

Reference yield:

: 288-13-1
NH-pyrazole

: 108-38-3,104809-90-7
m-xylene

: 84401-18-3
1-(2,4-dimethylphenyl)-(1H-pyrazole)

: 38581-14-5
1-(2,6-dimethylphenyl)-1H-pyrazole

Guidance literature:: With C₂₄H₄₂N₃⁽¹⁺⁾*ClO₄^(1-); lithium perchlorate; acetic acid; In acetonitrile; at 20 ℃; for 72h; Overall yield = 71 percent; Overall yield = 48.9 mg; Electrochemical reaction; Sealed tube; Irradiation;
DOI:10.1002/anie.201906381