(1R,2R,4S,5S,6S)-3,3-Bis-benzenesulfonyl-4-phenyl-tricyclo[4.2.1.0^2,5]non-7-ene

Base Information

• Chemical Name: (1R,2R,4S,5S,6S)-3,3-Bis-benzenesulfonyl-4-phenyl-tricyclo[4.2.1.0^2,5]non-7-ene
• CAS No.: 141831-97-2
• Molecular Formula: C₂₇H₂₄O₄S₂
• Molecular Weight: 476.617

Synonyms:(1R,2R,4S,5S,6S)-3,3-Bis-benzenesulfonyl-4-phenyl-tricyclo[4.2.1.0^2,5]non-7-ene

Chemical Property of (1R,2R,4S,5S,6S)-3,3-Bis-benzenesulfonyl-4-phenyl-tricyclo[4.2.1.0^2,5]non-7-ene

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Technology Process of (1R,2R,4S,5S,6S)-3,3-Bis-benzenesulfonyl-4-phenyl-tricyclo[4.2.1.0^2,5]non-7-ene

There total 1 articles about (1R,2R,4S,5S,6S)-3,3-Bis-benzenesulfonyl-4-phenyl-tricyclo[4.2.1.0^2,5]non-7-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1,1-bis(phenylsulfonyl)-2-phenylethene (39082-44-5) + quadricyclo[2.2.1.0.0]heptane (278-06-8) → (1R,2R,4S,5S,6S)-3,3-Bis-benzenesulfonyl-4-phenyl-tricyclo[4.2.1.02,5]non-7-ene (141831-97-2)

Guidance literature:

lithium perchlorate; In diethyl ether; at 40 - 50 ℃; for 24h; sonication;

DOI:10.1016/S0040-4020(01)92236-7

Reference yield: 95.0%

(1R,2R,4S,5S,6S)-3,3-Bis-benzenesulfonyl-4-phenyl-tricyclo[4.2.1.02,5]non-7-ene (141831-97-2) → (1S,2S,3S,5R,6R)-3-Phenyl-tricyclo[4.2.1.02,5]non-7-ene (141862-40-0)

Guidance literature:

With sodium dihydrogenphosphate; sodium amalgam; In methanol; for 12h; Ambient temperature;

DOI:10.1016/S0040-4020(01)92236-7

upstream raw materials:

1,1-bis(phenylsulfonyl)-2-phenylethene

quadricyclo[2.2.1.0.0]heptane

Downstream raw materials:

(1S,2S,3S,5R,6R)-3-Phenyl-tricyclo[4.2.1.0^2,5]non-7-ene

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