benzyl tetradec-13-enoate

Base Information

Chemical Name:benzyl tetradec-13-enoate
CAS No.:1574334-34-1
Molecular Formula:C₂₁H₃₂O₂
Molecular Weight:316.484
Hs Code.:

Synonyms:benzyl tetradec-13-enoate

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Chemical Property of benzyl tetradec-13-enoate

Chemical Property:

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Technology Process of benzyl tetradec-13-enoate

There total 6 articles about benzyl tetradec-13-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98008-53-8
11-(dimethyl-t-butylsilyloxy)undecyl bromide

: 1574334-34-1
benzyl tetradec-13-enoate

Guidance literature:: Multi-step reaction with 5 steps

1: copper(l) iodide / tetrahydrofuran / -78 - 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h

3: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 1 h / -60 - -50 °C

4: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol

5: toluene-4-sulfonic acid / toluene / Reflux

With sodium chlorite; copper(l) iodide; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; oxalyl dichloride; tetrabutyl ammonium fluoride; toluene-4-sulfonic acid; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane; water; toluene; tert-butyl alcohol;
DOI:10.1039/c3ob42364f

Reference yield:

: 85896-31-7
tetradec-13-enal

: 1574334-34-1
benzyl tetradec-13-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol

2: toluene-4-sulfonic acid / toluene / Reflux

With sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; toluene-4-sulfonic acid; In water; toluene; tert-butyl alcohol;
DOI:10.1039/c3ob42364f

Reference yield:

: 1225281-87-7
C₂₀H₄₂OSi

: 1574334-34-1
benzyl tetradec-13-enoate

Guidance literature:: Multi-step reaction with 4 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h

2: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 1 h / -60 - -50 °C

3: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol

4: toluene-4-sulfonic acid / toluene / Reflux

With sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; oxalyl dichloride; tetrabutyl ammonium fluoride; toluene-4-sulfonic acid; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane; water; toluene; tert-butyl alcohol;
DOI:10.1039/c3ob42364f