3-methoxy-4-aminopropiophenone

Base Information

Chemical Name:3-methoxy-4-aminopropiophenone
CAS No.:1410922-80-3
Molecular Formula:C₁₀H₁₃NO₂
Molecular Weight:179.219
Hs Code.:

Synonyms:3-methoxy-4-aminopropiophenone

Suppliers and Price of 3-methoxy-4-aminopropiophenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 3-methoxy-4-aminopropiophenone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-methoxy-4-aminopropiophenone

There total 3 articles about 3-methoxy-4-aminopropiophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 3-methoxy-4-nitropropiophenone

: 1410922-80-3
3-methoxy-4-aminopropiophenone

Guidance literature:: With 10% Pd/C; ammonium formate; In methanol; for 0.333333h; Inert atmosphere; Microwave irradiation;
DOI:10.3184/174751912X13418461206368

Reference yield:

: 3027-13-2
1-(3-methoxyphenyl)propan-2-one

: 1410922-80-3
3-methoxy-4-aminopropiophenone

Guidance literature:: Multi-step reaction with 4 steps

1: potassium hydroxide; hydrazine hydrate / diethylene glycol / 0.83 h / 112 - 180 °C / Microwave irradiation

2: copper(II) nitrate monohydrate; acetic anhydride / diethyl ether / 4 h / 20 °C

3: pyridinium chlorochromate / benzene / 24 h / Reflux

4: 10% Pd/C; ammonium formate / methanol / 0.33 h / Inert atmosphere; Microwave irradiation

With copper(II) nitrate monohydrate; 10% Pd/C; ammonium formate; acetic anhydride; hydrazine hydrate; pyridinium chlorochromate; potassium hydroxide; In methanol; diethyl ether; diethylene glycol; benzene; 1: |Wolff-Kishner Reduction;
DOI:10.3184/174751912X13418461206368

Reference yield:

: 62103-69-9
3-propylanisole

: 1410922-80-3
3-methoxy-4-aminopropiophenone

Guidance literature:: Multi-step reaction with 3 steps

1: copper(II) nitrate monohydrate; acetic anhydride / diethyl ether / 4 h / 20 °C

2: pyridinium chlorochromate / benzene / 24 h / Reflux

3: 10% Pd/C; ammonium formate / methanol / 0.33 h / Inert atmosphere; Microwave irradiation

With copper(II) nitrate monohydrate; 10% Pd/C; ammonium formate; acetic anhydride; pyridinium chlorochromate; In methanol; diethyl ether; benzene;
DOI:10.3184/174751912X13418461206368