3-(2-((bis(benzyloxy)phosphoryl)oxy)-4,6-dimethylphenyl)-3-methylbutanoic isobutyl carbonic anhydride

Base Information

Chemical Name:3-(2-((bis(benzyloxy)phosphoryl)oxy)-4,6-dimethylphenyl)-3-methylbutanoic isobutyl carbonic anhydride
CAS No.:247018-06-0
Molecular Formula:C₃₂H₃₉O₈P
Molecular Weight:582.631
Hs Code.:

Synonyms:3-(2-((bis(benzyloxy)phosphoryl)oxy)-4,6-dimethylphenyl)-3-methylbutanoic isobutyl carbonic anhydride

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Chemical Property of 3-(2-((bis(benzyloxy)phosphoryl)oxy)-4,6-dimethylphenyl)-3-methylbutanoic isobutyl carbonic anhydride

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Technology Process of 3-(2-((bis(benzyloxy)phosphoryl)oxy)-4,6-dimethylphenyl)-3-methylbutanoic isobutyl carbonic anhydride

There total 1 articles about 3-(2-((bis(benzyloxy)phosphoryl)oxy)-4,6-dimethylphenyl)-3-methylbutanoic isobutyl carbonic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 153910-62-4
3-(2-((bis(benzyloxy)phosphoryl)oxy)-4,6-dimethylphenyl)-3-methylbutanoic acid

: 543-27-1
isobutyl chloroformate

: 247018-06-0
3-(2-((bis(benzyloxy)phosphoryl)oxy)-4,6-dimethylphenyl)-3-methylbutanoic isobutyl carbonic anhydride

Guidance literature:: With 4-methyl-morpholine; In dichloromethane; at -10 ℃;
DOI:10.1016/S0960-894X(00)00183-9

Reference yield: 87.0%

: 158991-23-2
PD 154075

: 247018-06-0
3-(2-((bis(benzyloxy)phosphoryl)oxy)-4,6-dimethylphenyl)-3-methylbutanoic isobutyl carbonic anhydride

: [(R)-2-(1-{3-[2-(Bis-benzyloxy-phosphoryloxy)-4,6-dimethyl-phenyl]-3-methyl-butyryl}-1H-indol-3-yl)-1-methyl-1-((S)-1-phenyl-ethylcarbamoyl)-ethyl]-carbamic acid benzofuran-2-ylmethyl ester

Guidance literature:: PD 154075; With potassium hexamethylsilazane; In tetrahydrofuran; at -78 ℃;

3-(2-((bis(benzyloxy)phosphoryl)oxy)-4,6-dimethylphenyl)-3-methylbutanoic isobutyl carbonic anhydride; In tetrahydrofuran;
DOI:10.1016/S0960-894X(00)00183-9

Reference yield:

: 4-(5-(2,4-bis(trifluoromethyl)benzyl)-2-(2,6-diethylphenyl)-6,6-dimethyl-2,4,5,6-tetrahydropyrrolo[3,4-c]pyrazol-3-yl)-7-fluoro-1H-indole

: 247018-06-0
3-(2-((bis(benzyloxy)phosphoryl)oxy)-4,6-dimethylphenyl)-3-methylbutanoic isobutyl carbonic anhydride

: dibenzyl (2-(4-(4-(5-(2,4-bis(trifluoromethyl)benzyl)-2-(2,6-diethylphenyl)-6,6-dimethyl-2,4,5,6-tetrahydropyrrolo[3,4-c]pyrazol-3-yl)-7-fluoro-1H-indol-1-yl)-2-methyl-4-oxobutan-2-yl)-3,5-dimethylphenyl)phosphate

Guidance literature:: 4-(5-(2,4-bis(trifluoromethyl)benzyl)-2-(2,6-diethylphenyl)-6,6-dimethyl-2,4,5,6-tetrahydropyrrolo[3,4-c]pyrazol-3-yl)-7-fluoro-1H-indole; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.5h;

3-(2-((bis(benzyloxy)phosphoryl)oxy)-4,6-dimethylphenyl)-3-methylbutanoic isobutyl carbonic anhydride; In tetrahydrofuran; at -78 - 20 ℃; for 3h;