(2S,4S)-N-tert.-butoxycarbonyl-2-bis(2-methoxyphenyl)phosphinomethyl-4-bis(4-methoxyphenyl)phosphinopyrrolidine

Base Information

Chemical Name:(2S,4S)-N-tert.-butoxycarbonyl-2-bis(2-methoxyphenyl)phosphinomethyl-4-bis(4-methoxyphenyl)phosphinopyrrolidine
CAS No.:120481-30-3
Molecular Formula:C₃₈H₄₅NO₆P₂
Molecular Weight:673.726
Hs Code.:

Synonyms:(2S,4S)-N-tert.-butoxycarbonyl-2-bis(2-methoxyphenyl)phosphinomethyl-4-bis(4-methoxyphenyl)phosphinopyrrolidine

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Chemical Property of (2S,4S)-N-tert.-butoxycarbonyl-2-bis(2-methoxyphenyl)phosphinomethyl-4-bis(4-methoxyphenyl)phosphinopyrrolidine

Chemical Property:

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Technology Process of (2S,4S)-N-tert.-butoxycarbonyl-2-bis(2-methoxyphenyl)phosphinomethyl-4-bis(4-methoxyphenyl)phosphinopyrrolidine

There total 9 articles about (2S,4S)-N-tert.-butoxycarbonyl-2-bis(2-methoxyphenyl)phosphinomethyl-4-bis(4-methoxyphenyl)phosphinopyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2S,4S)-2-bis(2-methoxyphenyl)phosphinomethyl-4-bis(4-methoxyphenyl)phosphinopyrrolidine

: 24424-99-5
di-tert-butyl dicarbonate

: 120481-30-3
(2S,4S)-N-tert.-butoxycarbonyl-2-bis(2-methoxyphenyl)phosphinomethyl-4-bis(4-methoxyphenyl)phosphinopyrrolidine

Guidance literature:: With triethylamine; In dichloromethane;

Reference yield:

: 39864-55-6
Lithium-di-(p-anisyl)-phosphid

: 120481-30-3
(2S,4S)-N-tert.-butoxycarbonyl-2-bis(2-methoxyphenyl)phosphinomethyl-4-bis(4-methoxyphenyl)phosphinopyrrolidine

Guidance literature:: Multi-step reaction with 5 steps

1: 2.) 10percent H₂O₂

2: 1.) n-Bu₄NF

3: 2.) 10percent H₂O₂

4: 100 percent / CF₃COOH

5: 1.) HSiCl₃-NEt₃

With HSiCl₃-NEt₃; tetrabutyl ammonium fluoride; dihydrogen peroxide; trifluoroacetic acid;

Reference yield:

: 61478-26-0
tert-butyl (2S,4R)-4-hydroxy-2-hydroxymethyl-pyrrolidine-1-carboxylate

: 120481-30-3
(2S,4S)-N-tert.-butoxycarbonyl-2-bis(2-methoxyphenyl)phosphinomethyl-4-bis(4-methoxyphenyl)phosphinopyrrolidine

Guidance literature:: Multi-step reaction with 6 steps

2: 2.) 10percent H₂O₂

3: 1.) n-Bu₄NF

4: 2.) 10percent H₂O₂

5: 100 percent / CF₃COOH

6: 1.) HSiCl₃-NEt₃

With HSiCl₃-NEt₃; tetrabutyl ammonium fluoride; dihydrogen peroxide; trifluoroacetic acid;