(3S,4R,6R)-1-benzyl-6-O-benzyl-3,4-O-cyclohexylidene-3,4,6-trihydroxyazepane

Base Information

Chemical Name:(3S,4R,6R)-1-benzyl-6-O-benzyl-3,4-O-cyclohexylidene-3,4,6-trihydroxyazepane
CAS No.:943032-30-2
Molecular Formula:C₂₆H₃₃NO₃
Molecular Weight:407.553
Hs Code.:

Synonyms:(3S,4R,6R)-1-benzyl-6-O-benzyl-3,4-O-cyclohexylidene-3,4,6-trihydroxyazepane

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Chemical Property of (3S,4R,6R)-1-benzyl-6-O-benzyl-3,4-O-cyclohexylidene-3,4,6-trihydroxyazepane

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Technology Process of (3S,4R,6R)-1-benzyl-6-O-benzyl-3,4-O-cyclohexylidene-3,4,6-trihydroxyazepane

There total 2 articles about (3S,4R,6R)-1-benzyl-6-O-benzyl-3,4-O-cyclohexylidene-3,4,6-trihydroxyazepane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (1R,4S,5R)-1-O-benzyl-4,5-O-cyclohexylidene-1,4,5-trihydroxy-2-cyclohexene

: 943032-30-2
(3S,4R,6R)-1-benzyl-6-O-benzyl-3,4-O-cyclohexylidene-3,4,6-trihydroxyazepane

Guidance literature:: Multi-step reaction with 3 steps

1.1: 73 percent / NaIO₄ / RuCl₃ / ethyl acetate; acetonitrile; aq. phosphate buffer / 0.17 h / 0 °C / pH 7

2.1: NaIO₄ / methanol

2.2: aq. NaHCO₃ / ethyl acetate

3.1: NaBH(OAc)3 / CH₂Cl₂ / 20 °C

With sodium periodate; sodium tris(acetoxy)borohydride; ruthenium trichloride; In methanol; phosphate buffer; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1021/jo070058x

Reference yield:

: 943032-28-8
C₁₉H₂₆O₅

: 943032-30-2
(3S,4R,6R)-1-benzyl-6-O-benzyl-3,4-O-cyclohexylidene-3,4,6-trihydroxyazepane

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaIO₄ / methanol

1.2: aq. NaHCO₃ / ethyl acetate

2.1: NaBH(OAc)3 / CH₂Cl₂ / 20 °C

With sodium periodate; sodium tris(acetoxy)borohydride; In methanol; dichloromethane;
DOI:10.1021/jo070058x