Dimethyl-(2S, 3aR, 8aS)-8-acetyl-1,2,3,3a,8a-hexahydropyrrolo[2,3]indol-1,2-dicarboxylate

Base Information

Chemical Name:Dimethyl-(2S, 3aR, 8aS)-8-acetyl-1,2,3,3a,8a-hexahydropyrrolo[2,3]indol-1,2-dicarboxylate
CAS No.:79465-83-1
Molecular Formula:C₁₆H₁₈N₂O₅
Molecular Weight:318.329
Hs Code.:
Mol file:79465-83-1.mol

Synonyms:Pyrrolo[2,3-b]indole-1,2(2H)-dicarboxylicacid, 8-acetyl-3,3a,8,8a-tetrahydro-, dimethyl ester, (2a,3ab,8ab)- (9CI); Pyrrolo[2,3-b]indole-1,2(2H)-dicarboxylic acid,8-acetyl-3,3a,8,8a-tetrahydro-, dimethyl ester, (2a,3ab,8ab)-(?à)-

Suppliers and Price of Dimethyl-(2S, 3aR, 8aS)-8-acetyl-1,2,3,3a,8a-hexahydropyrrolo[2,3]indol-1,2-dicarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of Dimethyl-(2S, 3aR, 8aS)-8-acetyl-1,2,3,3a,8a-hexahydropyrrolo[2,3]indol-1,2-dicarboxylate

Chemical Property:

PSA：76.15000
LogP:1.47940

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Dimethyl-(2S, 3aR, 8aS)-8-acetyl-1,2,3,3a,8a-hexahydropyrrolo[2,3]indol-1,2-dicarboxylate

There total 4 articles about Dimethyl-(2S, 3aR, 8aS)-8-acetyl-1,2,3,3a,8a-hexahydropyrrolo[2,3]indol-1,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66377-68-2
N_b-methoxycarbonyl-DL-tryptophan methyl ester

: 67811-39-6,79465-83-1,79465-84-2,79465-85-3,79465-86-4
DL-(2β,3aα,8aα)-8-acetyl-1,2-dimethoxycarbonyl-1,2,3,3a,8,8a-hexahydropyrrolo<2,3-b>indole

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / 85percent phosphoric acid / 3 h / Ambient temperature

2: pyridine

With phosphoric acid; In pyridine;
DOI:10.1016/S0040-4020(01)92088-5

Reference yield:

: 108-24-7
acetic anhydride

: 67811-38-5,79465-82-0,79465-87-5,136088-17-0,146235-39-4
DL-(2β,3aα,8aα)-1,2,3,3a,8,8a-hexahydro-1,2-dimethoxycarbonylpyrrolo<2,3-b>indole

: 67811-39-6,79465-83-1,79465-84-2,79465-85-3,79465-86-4
DL-(2β,3aα,8aα)-8-acetyl-1,2-dimethoxycarbonyl-1,2,3,3a,8,8a-hexahydropyrrolo<2,3-b>indole

Guidance literature:: In pyridine;
DOI:10.1016/S0040-4020(01)92088-5

Reference yield:

: 66377-68-2
N_b-methoxycarbonyl-DL-tryptophan methyl ester

: 108-24-7
acetic anhydride

: 67811-39-6,79465-83-1,79465-84-2,79465-85-3,79465-86-4
DL-(2β,3aα,8aα)-8-acetyl-1,2-dimethoxycarbonyl-1,2,3,3a,8,8a-hexahydropyrrolo<2,3-b>indole

: 67811-39-6,79465-83-1,79465-84-2,79465-85-3,79465-86-4
DL-(2β,3aβ,8aβ)-8-acetyl-1,2-dimethoxycarbonyl-1,2,3,3a,8,8a-hexahydropyrrolo<2,3-b>indole

Guidance literature:: With phosphoric acid; Product distribution; 1.) RT, 1.5h; 2.) pyridine, RT; variation of acids, reaction times and temperatures in the first step;
DOI:10.1016/S0040-4020(01)92088-5