1,3-Dioxolan-2-one,4-ethenyl-5-(1-methylethyl)-,(4S,5S)-(9CI)

Base Information

Chemical Name:1,3-Dioxolan-2-one,4-ethenyl-5-(1-methylethyl)-,(4S,5S)-(9CI)
CAS No.:790300-34-4
Molecular Formula:C₈H₁₂O₃
Molecular Weight:156.181
Hs Code.:
Mol file:790300-34-4.mol

Synonyms:1,3-Dioxolan-2-one,4-ethenyl-5-(1-methylethyl)-,(4S,5S)-(9CI)

Suppliers and Price of 1,3-Dioxolan-2-one,4-ethenyl-5-(1-methylethyl)-,(4S,5S)-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-Dioxolan-2-one,4-ethenyl-5-(1-methylethyl)-,(4S,5S)-(9CI)

Chemical Property:

PSA：35.53000
LogP:1.73240

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 1,3-Dioxolan-2-one,4-ethenyl-5-(1-methylethyl)-,(4S,5S)-(9CI)

There total 13 articles about 1,3-Dioxolan-2-one,4-ethenyl-5-(1-methylethyl)-,(4S,5S)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 790300-31-1
Carbonic acid tert-butyl ester (Z)-(S)-4-hydroxy-5-methyl-hex-2-enyl ester

: 790300-34-4
(S,S)-4-isopropyl-5-vinyl-1,3-dioxolan-2-one

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; at 20 ℃; for 0.25h;
DOI:10.1021/jo048985g

Reference yield: 70.0%

: trans-4-isopropyl-2-tosylimino-5-vinyl-1,3-dioxolane

: 790300-34-4
4,5-trans-4-(1-methylethenyl)-5-ethenyl-1,3-dioxolan-2-one

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; water; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1002/ejoc.201200378

Reference yield:

: 790300-24-2
tert-butyl (S)-4-hydroxy-5-methylhex-2-ynyl carbonate

: 790300-34-4
(S,S)-4-isopropyl-5-vinyl-1,3-dioxolan-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / H₂; quinoline / Pd/CaCO₃ poisoned with lead / ethyl acetate / 0.5 h

2: 87 percent / Pd(PPh₃)4 / CH₂Cl₂ / 0.25 h / 20 °C

With quinoline; hydrogen; Lindlar's catalyst; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; ethyl acetate;
DOI:10.1021/jo048985g