C₅₂H₇₃N₃O₁₅

Base Information

Chemical Name:C₅₂H₇₃N₃O₁₅
CAS No.:1369430-93-2
Molecular Formula:C₅₂H₇₃N₃O₁₅
Molecular Weight:980.163
Hs Code.:

C<sub>52</sub>H<sub>73</sub>N<sub>3</sub>O<sub>15</sub>

Synonyms:C₅₂H₇₃N₃O₁₅

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Chemical Property of C₅₂H₇₃N₃O₁₅

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Technology Process of C₅₂H₇₃N₃O₁₅

There total 24 articles about C₅₂H₇₃N₃O₁₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1240304-81-7
C₁₃H₂₇N₃O₃

: 1369430-79-4
C₃₉H₄₈O₁₃

: 1369430-93-2
C₅₂H₇₃N₃O₁₅

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 11h;

Reference yield:

: 1240304-83-9
C₂₁H₃₃N₃O₅

: 1369430-93-2
C₅₂H₇₃N₃O₁₅

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium(II) hydroxide / methanol / 4.5 h / 20 °C

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 11 h / 20 °C

With hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; palladium(II) hydroxide; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 1240304-54-4
1,5-dibromo-2-(methoxymethoxy)-4-(propan-2-yl)benzene

: 1369430-93-2
C₅₂H₇₃N₃O₁₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.92 h / -86 - -74 °C / Inert atmosphere

1.2: 1.47 h / -86 - -74 °C

2.1: methanesulfonic acid / methanol / 1 h / Reflux

3.1: acetic anhydride; N-ethyl-N,N-diisopropylamine / dmap / tetrahydrofuran / 21 h / 20 °C

4.1: trimethylsilyl trifluoromethanesulfonate; tert-butyldimethylsilane / water; acetonitrile / 1.5 h / Cooling

4.2: 0.42 h / Cooling

5.1: triethylamine / palladium diacetate; tris-(o-tolyl)phosphine / acetonitrile / 3 h / Inert atmosphere; Reflux

6.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 11 h / 20 °C

With n-butyllithium; methanesulfonic acid; trimethylsilyl trifluoromethanesulfonate; tert-butyldimethylsilane; acetic anhydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; dmap; palladium diacetate; tris-(o-tolyl)phosphine; In tetrahydrofuran; methanol; hexane; water; N,N-dimethyl-formamide; acetonitrile; 5.1: Heck Reaction;