C₁₇H₁₆O₄

Base Information

Chemical Name:C₁₇H₁₆O₄
CAS No.:1447648-22-7
Molecular Formula:C₁₇H₁₆O₄
Molecular Weight:284.312
Hs Code.:

C<sub>17</sub>H<sub>16</sub>O<sub>4</sub>

Synonyms:C₁₇H₁₆O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₇H₁₆O₄

Chemical Property:

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Technology Process of C₁₇H₁₆O₄

There total 14 articles about C₁₇H₁₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: C₃₀H₃₈O₆Si

: 1447648-21-6
C₁₇H₁₆O₄

: 1447648-22-7
C₁₇H₁₆O₄

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -78 - 0 ℃; for 4h; Molecular sieve; Inert atmosphere;
DOI:10.1002/asia.201300362

Reference yield: 10.0%

: C₃₀H₃₈O₆Si

: 1447648-22-7
C₁₇H₁₆O₄

Guidance literature:: With zinc(II) chloride; In dichloromethane; at -78 - -30 ℃; for 13h; Molecular sieve; Inert atmosphere;
DOI:10.1002/asia.201300362

Reference yield:

: 1447648-17-0
C₂₃H₃₂O₅Si

: 1447648-22-7
C₁₇H₁₆O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid; tetrabutyl ammonium fluoride / tetrahydrofuran / 22 h / 0 - 20 °C / Inert atmosphere

2.1: N,N,N,N,-tetramethylethylenediamine / dichloromethane / 0.6 h / 0 °C / Inert atmosphere

3.1: lithium hexamethyldisilazane / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

3.2: -78 - -20 °C / Inert atmosphere

4.1: zinc(II) chloride / dichloromethane / 13 h / -78 - -30 °C / Molecular sieve; Inert atmosphere

With N,N,N,N,-tetramethylethylenediamine; tetrabutyl ammonium fluoride; acetic acid; zinc(II) chloride; lithium hexamethyldisilazane; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1002/asia.201300362