N,N'-bis(phenylsulfonyl)sulfoxylic diamide

Base Information

• Chemical Name: N,N'-bis(phenylsulfonyl)sulfoxylic diamide
• CAS No.: 81955-02-4
• Molecular Formula: C₁₂H₁₂N₂O₄S₃
• Molecular Weight: 344.436
• Mol file: 81955-02-4.mol

Synonyms:N,N'-bis(phenylsulfonyl)sulfoxylic diamide

Chemical Property of N,N'-bis(phenylsulfonyl)sulfoxylic diamide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of N,N'-bis(phenylsulfonyl)sulfoxylic diamide

There total 2 articles about N,N'-bis(phenylsulfonyl)sulfoxylic diamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

N,N'-bis(phenylsulfonyl)sulfur diimide (667-20-9) → di(benzothiazol-2-yl)disulfide (120-78-5) + N,N'-bis(phenylsulfonyl)sulfoxylic diamide (81955-02-4)

Guidance literature:

With 2-Mercaptobenzothiazole; In benzene; for 8h; Heating;

Reference yield: 89.0%

N,N'-bis(phenylsulfonyl)sulfur diimide (667-20-9) → di(p-tolyl) disulfide (103-19-5) + N,N'-bis(phenylsulfonyl)sulfoxylic diamide (81955-02-4)

Guidance literature:

With para-thiocresol; In benzene; for 4h; Ambient temperature; p-ClC₆H₄SH as reagent.;

Reference yield: 100.0%

dimedone (126-81-8) + N,N'-bis(phenylsulfonyl)sulfoxylic diamide (81955-02-4) → benzenesulfonamide (98-10-2) + 4',4',6,6-tetramethyl-6,7-dihydro-2'H,6'H-spiro[1,3-benzoxathiol-2,1'-cyclohexan]-2',4,6'(5H)-trion (56995-07-4) + bis(4,4-dimethyl-2,6-dioxo-1-cyclohexyl) sulfide (3359-52-2)

Guidance literature:

In benzene; at 20 ℃; for 6h;

upstream raw materials:

N,N'-bis(phenylsulfonyl)sulfur diimide

Downstream raw materials:

morpholinium morpholidobis(phenylsulfonamido)sulfite

benzenesulfonamide

4',4',6,6-tetramethyl-6,7-dihydro-2'H,6'H-spiro[1,3-benzoxathiol-2,1'-cyclohexan]-2',4,6'(5H)-trion

bis(4,4-dimethyl-2,6-dioxo-1-cyclohexyl) sulfide