N-n-hexyl-5,6,8,9-tetrahydro-7-phenyldibenzacridinium trifluoromethanesulfonate

Base Information

• Chemical Name: N-n-hexyl-5,6,8,9-tetrahydro-7-phenyldibenzacridinium trifluoromethanesulfonate
• CAS No.: 76017-70-4
• Molecular Formula: CF₃O₃S*C₃₃H₃₄N
• Molecular Weight: 593.71
• Mol file: 76017-70-4.mol

Synonyms:N-n-hexyl-5,6,8,9-tetrahydro-7-phenyldibenzacridinium trifluoromethanesulfonate

Chemical Property of N-n-hexyl-5,6,8,9-tetrahydro-7-phenyldibenzacridinium trifluoromethanesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-n-hexyl-5,6,8,9-tetrahydro-7-phenyldibenzacridinium trifluoromethanesulfonate

There total 3 articles about N-n-hexyl-5,6,8,9-tetrahydro-7-phenyldibenzacridinium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

hexan-1-amine (111-26-2) + 5,6,8,9-tetrahydro-7-phenyldibenzoxanthyilium triflouromethanesulphonate (73377-38-5) → N-n-hexyl-5,6,8,9-tetrahydro-7-phenyldibenzacridinium trifluoromethanesulfonate (76017-70-4)

Guidance literature:

In diethyl ether; at 20 ℃; for 6h;

DOI:10.1021/jo00139a024

Reference yield:

2-benzylidene-1-tetralone (6261-32-1) → N-n-hexyl-5,6,8,9-tetrahydro-7-phenyldibenzacridinium trifluoromethanesulfonate (76017-70-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 51 percent / 4 h / steam bath

2: 88 percent / diethyl ether / 12 h / 20 °C

In diethyl ether;

DOI:10.1039/P19810000661

Reference yield:

3,4-dihydronaphthalene-1(2H)-one (529-34-0) → N-n-hexyl-5,6,8,9-tetrahydro-7-phenyldibenzacridinium trifluoromethanesulfonate (76017-70-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 51 percent / 4 h / steam bath

2: 88 percent / diethyl ether / 12 h / 20 °C

In diethyl ether;

DOI:10.1039/P19810000661

upstream raw materials:

hexan-1-amine

5,6,8,9-tetrahydro-7-phenyldibenzoxanthyilium triflouromethanesulphonate

2-benzylidene-1-tetralone

3,4-dihydronaphthalene-1(2H)-one

Downstream raw materials:

5,6,8,9-tetrahydro-7-phenyldibenzolacridine

ethyl 2-acetyloctanoate

1-hexene

cis-2-hexene