2-<<4-(2-carbomethoxyetyl)phenethyl>amino>adenosine-5'-N-ethylcarboxamide hydrochloride

Base Information

Chemical Name:2-<<4-(2-carbomethoxyetyl)phenethyl>amino>adenosine-5'-N-ethylcarboxamide hydrochloride
CAS No.:127258-46-2
Molecular Formula:C₂₄H₃₁N₇O₆*ClH
Molecular Weight:550.014
Hs Code.:

Synonyms:2-<<4-(2-carbomethoxyetyl)phenethyl>amino>adenosine-5'-N-ethylcarboxamide hydrochloride

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Chemical Property of 2-<<4-(2-carbomethoxyetyl)phenethyl>amino>adenosine-5'-N-ethylcarboxamide hydrochloride

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Technology Process of 2-<<4-(2-carbomethoxyetyl)phenethyl>amino>adenosine-5'-N-ethylcarboxamide hydrochloride

There total 9 articles about 2-<<4-(2-carbomethoxyetyl)phenethyl>amino>adenosine-5'-N-ethylcarboxamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16532-79-9
4-Bromophenylacetonitrile

: 127258-46-2
2-<<4-(2-carbomethoxyetyl)phenethyl>amino>adenosine-5'-N-ethylcarboxamide hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: 105 g / Pd(OAc)2, tri-o-tolylphosphine / triethylamine / 6 h / Heating

2: 84 percent / 1 N HCl, H₂ / 10percent Pd/C / propan-2-ol / 7 h / 2585.7 Torr / Heating

3: 55 percent / 3 h / 130 °C

4: 96 percent / 1 N HCl / 1 h / 65 °C

5: 1.) propylene oxide, EtOH / 1.) THF, 2.) ether, RT, 3 h

With hydrogenchloride; palladium diacetate; ethanol; hydrogen; tris-(o-tolyl)phosphine; methyloxirane; palladium on activated charcoal; In triethylamine; isopropyl alcohol;
DOI:10.1021/jm00169a015

Reference yield:

: 120225-74-3
(E)-tert-butyl 3-(4-(cyanomethyl)phenyl)acrylate

: 127258-46-2
2-<<4-(2-carbomethoxyetyl)phenethyl>amino>adenosine-5'-N-ethylcarboxamide hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / 1 N HCl, H₂ / 10percent Pd/C / propan-2-ol / 7 h / 2585.7 Torr / Heating

2: 55 percent / 3 h / 130 °C

3: 96 percent / 1 N HCl / 1 h / 65 °C

4: 1.) propylene oxide, EtOH / 1.) THF, 2.) ether, RT, 3 h

With hydrogenchloride; ethanol; hydrogen; methyloxirane; palladium on activated charcoal; In isopropyl alcohol;
DOI:10.1021/jm00169a015

Reference yield:

: 24639-06-3
((3aR,4R,6R,6aR)-6-(6-amino-2-chloro-9H-purin-9-yl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methanol

: 127258-46-2
2-<<4-(2-carbomethoxyetyl)phenethyl>amino>adenosine-5'-N-ethylcarboxamide hydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1: 74 percent / aq. KOH, KMnO₄ / H₂O / 72 h

2: SOCl₂ / dimethylformamide / 2 h / 50 °C

3: CH₂Cl₂ / 1 h / Ambient temperature

4: 55 percent / 3 h / 130 °C

5: 96 percent / 1 N HCl / 1 h / 65 °C

6: 1.) propylene oxide, EtOH / 1.) THF, 2.) ether, RT, 3 h

With hydrogenchloride; potassium hydroxide; potassium permanganate; thionyl chloride; ethanol; methyloxirane; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00169a015