2-(2,5-dimethyl-1H-pyrrol-1-yl)benzenethiol

Base Information

Chemical Name:2-(2,5-dimethyl-1H-pyrrol-1-yl)benzenethiol
CAS No.:88613-63-2
Molecular Formula:C₁₂H₁₃NS
Molecular Weight:203.308
Hs Code.:

Synonyms:2-(2,5-dimethyl-1H-pyrrol-1-yl)benzenethiol

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Chemical Property of 2-(2,5-dimethyl-1H-pyrrol-1-yl)benzenethiol

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Technology Process of 2-(2,5-dimethyl-1H-pyrrol-1-yl)benzenethiol

There total 2 articles about 2-(2,5-dimethyl-1H-pyrrol-1-yl)benzenethiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 110-13-4
2,5-hexanedione

: 137-07-5
2-amino-benzenethiol

: 88613-63-2
2-(2,5-dimethyl-1H-pyrrol-1-yl)benzenethiol

Guidance literature:: With amberlite IR 120 acidic resin; at 20 ℃; for 0.6h; Neat (no solvent);
DOI:10.1080/00397911.2010.540766

Reference yield:

: 88613-63-2
2-(2,5-dimethyl-1H-pyrrol-1-yl)benzenethiol

Guidance literature:: Acetonylaceton, 2-Mercapto-anilin, Siedetemp.;

Reference yield: 86.0%

: 88613-63-2
2-(2,5-dimethyl-1H-pyrrol-1-yl)benzenethiol

: 2001-45-8
tetraphenyl phosphonium chloride

: 10108-64-2
cadmium(II) chloride

: [Ph₄P]2[Cd(N-(2-phenylthiolato)-2,5-dimethylpyrrole)4]

Guidance literature:: With Et₃N; In N,N-dimethyl-formamide; isopropyl alcohol; inert atmosphere; addn. of Et3N, Ph4PCl and metal salt to ligand (in DMF/i-PrOH=1:9 v/v), stirring overnight; collection, drying (vac.); can be recrystallized (DMF/i-PrOH=1/10 v/v, 0.°C, 24 h); elem. anal.;
DOI:10.1016/S0020-1693(98)00351-X