C₂₂H₂₈O₄

Base Information

Chemical Name:C₂₂H₂₈O₄
CAS No.:1196977-67-9
Molecular Formula:C₂₂H₂₈O₄
Molecular Weight:356.462
Hs Code.:

C<sub>22</sub>H<sub>28</sub>O<sub>4</sub>

Synonyms:C₂₂H₂₈O₄

Suppliers and Price of C₂₂H₂₈O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₈O₄

Chemical Property:

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Technology Process of C₂₂H₂₈O₄

There total 6 articles about C₂₂H₂₈O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1196977-66-8
C₂₂H₃₀O₄

: 1196977-67-9
C₂₂H₂₈O₄

Guidance literature:: With sulfur trioxide pyridine complex; N-ethyl-N,N-diisopropylamine; In dichloromethane; dimethyl sulfoxide; at 0 ℃;
DOI:10.1055/s-0029-1217707

Reference yield:

: 1534384-84-3
C₂₂H₂₈O₄

: 1196977-67-9
C₂₂H₂₈O₄

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / dichloromethane / 1 h / 0 °C

2: oxalyl dichloride; triethylamine; dimethyl sulfoxide / dichloromethane / 3 h / -78 °C

With oxalyl dichloride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; In dichloromethane; 2: |Swern Oxidation;
DOI:10.1039/c3ra44354j

Reference yield:

: C₁₈H₂₈O₅

: 1196977-67-9
C₂₂H₂₈O₄

Guidance literature:: Multi-step reaction with 5 steps

1: sodium periodate / tetrahydrofuran; water / 0.5 h / 0 °C

2: sodium tetrahydroborate / methanol / 0.5 h / 0 °C

3: sodium hydride / tetrahydrofuran / 4 h / 0 - 20 °C

4: diisobutylaluminium hydride / dichloromethane / 1 h / 0 °C

5: oxalyl dichloride; triethylamine; dimethyl sulfoxide / dichloromethane / 3 h / -78 °C

With sodium tetrahydroborate; sodium periodate; oxalyl dichloride; sodium hydride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; 5: |Swern Oxidation;
DOI:10.1039/c3ra44354j