2-[1-(Methoxycarbonyl-hydrazono)-ethyl]-3-(triphenyl-λ⁵-phosphanylidene)-succinic acid 1-tert-butyl ester 4-methyl ester

Base Information

• Chemical Name: 2-[1-(Methoxycarbonyl-hydrazono)-ethyl]-3-(triphenyl-λ⁵-phosphanylidene)-succinic acid 1-tert-butyl ester 4-methyl ester
• CAS No.: 130649-25-1
• Molecular Formula: C₃₁H₃₅N₂O₆P
• Molecular Weight: 562.602

Synonyms:2-[1-(Methoxycarbonyl-hydrazono)-ethyl]-3-(triphenyl-λ⁵-phosphanylidene)-succinic acid 1-tert-butyl ester 4-methyl ester

Chemical Property of 2-[1-(Methoxycarbonyl-hydrazono)-ethyl]-3-(triphenyl-λ⁵-phosphanylidene)-succinic acid 1-tert-butyl ester 4-methyl ester

Chemical Property:

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Technology Process of 2-[1-(Methoxycarbonyl-hydrazono)-ethyl]-3-(triphenyl-λ⁵-phosphanylidene)-succinic acid 1-tert-butyl ester 4-methyl ester

There total 1 articles about 2-[1-(Methoxycarbonyl-hydrazono)-ethyl]-3-(triphenyl-λ⁵-phosphanylidene)-succinic acid 1-tert-butyl ester 4-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

C10H16N2O4 (130649-44-4) + methyl (triphenylphosphoranylidene)acetate (21204-67-1,2605-67-6) → 2-[1-(Methoxycarbonyl-hydrazono)-ethyl]-3-(triphenyl-λ5-phosphanylidene)-succinic acid 1-tert-butyl ester 4-methyl ester (130649-25-1)

Guidance literature:

In tetrahydrofuran; at -20 ℃;

DOI:10.1016/S0040-4020(01)87767-X

Reference yield: 74.0%

2-[1-(Methoxycarbonyl-hydrazono)-ethyl]-3-(triphenyl-λ5-phosphanylidene)-succinic acid 1-tert-butyl ester 4-methyl ester (130649-25-1) → C30H31N2O5P

Guidance literature:

In methanol; for 8h; Heating;

DOI:10.1016/S0040-4020(01)87767-X

upstream raw materials:

C₁₀H₁₆N₂O₄

methyl (triphenylphosphoranylidene)acetate

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