2-Hexenoic acid, 5-(1-ethoxyethoxy)-, (2-trimethylsilyl)ethyl ester

Base Information

Chemical Name:2-Hexenoic acid, 5-(1-ethoxyethoxy)-, (2-trimethylsilyl)ethyl ester
CAS No.:79414-16-7
Molecular Formula:C₁₅H₃₀O₄Si
Molecular Weight:302.486
Hs Code.:
Mol file:79414-16-7.mol

Synonyms:2-Hexenoic acid, 5-(1-ethoxyethoxy)-, (2-trimethylsilyl)ethyl ester

Suppliers and Price of 2-Hexenoic acid, 5-(1-ethoxyethoxy)-, (2-trimethylsilyl)ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of 2-Hexenoic acid, 5-(1-ethoxyethoxy)-, (2-trimethylsilyl)ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 2-Hexenoic acid, 5-(1-ethoxyethoxy)-, (2-trimethylsilyl)ethyl ester

There total 4 articles about 2-Hexenoic acid, 5-(1-ethoxyethoxy)-, (2-trimethylsilyl)ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 79-08-3
bromoacetic acid

: 79414-15-6
2-(triphenyl-λ5-phosphine ylide) 2-(trimethylsilyl)ethyl acetate

: 79414-16-7
(S)-(2E)-5-(1'-Aethoxyaethoxy)-2-hexensaeure-<(2'-trimethylsilyl)aethyl>ester

Guidance literature:: In N,N-dimethyl-formamide; toluene; Ambient temperature;
DOI:10.1002/hlca.19810640523

Reference yield:

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 79414-16-7
(S)-(2E)-5-(1'-Aethoxyaethoxy)-2-hexensaeure-<(2'-trimethylsilyl)aethyl>ester

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / 4-(N,N-dimethylamino)pyridine, N,N-dicyclohexyl-carbodiimide / CH₂Cl₂ / 1 h / 0 °C

2: 91 percent / benzene / 16 h / Ambient temperature

3: 1 N KOH / CH₂Cl₂ / 0.03 h / 0 °C

4: 91 percent / toluene; dimethylformamide / Ambient temperature

With dmap; potassium hydroxide; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide; toluene; benzene;
DOI:10.1002/hlca.19810640523

Reference yield:

: 79414-13-4
trimethylsilylethyl bromoacetate

: 79414-16-7
(S)-(2E)-5-(1'-Aethoxyaethoxy)-2-hexensaeure-<(2'-trimethylsilyl)aethyl>ester

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / benzene / 16 h / Ambient temperature

2: 1 N KOH / CH₂Cl₂ / 0.03 h / 0 °C

3: 91 percent / toluene; dimethylformamide / Ambient temperature

With potassium hydroxide; In dichloromethane; N,N-dimethyl-formamide; toluene; benzene;
DOI:10.1002/hlca.19810640523