cyclopentadienyl(1,4-dimethyl-1,4-dibora-2,5-cyclohexadiene)cobalt

Base Information

• Chemical Name: cyclopentadienyl(1,4-dimethyl-1,4-dibora-2,5-cyclohexadiene)cobalt
• CAS No.: 75039-09-7
• Molecular Formula: C₁₁H₁₅B₂Co
• Molecular Weight: 227.855
• Mol file: 75039-09-7.mol

Synonyms:cyclopentadienyl(1,4-dimethyl-1,4-dibora-2,5-cyclohexadiene)cobalt

Chemical Property of cyclopentadienyl(1,4-dimethyl-1,4-dibora-2,5-cyclohexadiene)cobalt

Chemical Property:

Purity/Quality:

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Technology Process of cyclopentadienyl(1,4-dimethyl-1,4-dibora-2,5-cyclohexadiene)cobalt

There total 1 articles about cyclopentadienyl(1,4-dimethyl-1,4-dibora-2,5-cyclohexadiene)cobalt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

dicarbonylcyclopentadienylcobalt (12078-25-0,12078-23-8) + (ferrocenyl)dibromoborane + 1,1,4,4-tetramethyl-1,4-distanna-2,5-cyclohexadiene (66376-35-0) → ferrocene (102-54-5,55404-68-7) + cyclopentadienyl(1,4-dimethyl-1,4-dibora-2,5-cyclohexadiene)cobalt (75039-09-7)

Guidance literature:

With CH₃OH; CH₃MgI; In toluene; byproducts: CO; Sn compd. treated with Fe complex in CS2, then with CH3OH in toluene, Co complex added, heated to 80°C for 1 h, chromd. (Al2O3, CH2Cl2, CH2Cl2/MeOH), evapd. (vac.), stirred for 1 h with CH3MgI in ether at room temp.; hydrolyzed with moist Al2O3 at -80°C, evapd. (vac.), chromd. (Al2O3, pentane), concd., crystd. at -80°C; elem. anal.;

DOI:10.1016/S0022-328X(00)81234-6

upstream raw materials:

dicarbonylcyclopentadienylcobalt

1,1,4,4-tetramethyl-1,4-distanna-2,5-cyclohexadiene