methyl 3-(3,4-dihydro-5-phenyl-2H-pyrano[3,2-c]quinolin-9-yl)propanoate

Base Information

• Chemical Name: methyl 3-(3,4-dihydro-5-phenyl-2H-pyrano[3,2-c]quinolin-9-yl)propanoate
• CAS No.: 1185886-13-8
• Molecular Formula: C₂₂H₂₁NO₃
• Molecular Weight: 347.414

Synonyms:methyl 3-(3,4-dihydro-5-phenyl-2H-pyrano[3,2-c]quinolin-9-yl)propanoate

Chemical Property of methyl 3-(3,4-dihydro-5-phenyl-2H-pyrano[3,2-c]quinolin-9-yl)propanoate

Chemical Property:

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Technology Process of methyl 3-(3,4-dihydro-5-phenyl-2H-pyrano[3,2-c]quinolin-9-yl)propanoate

There total 2 articles about methyl 3-(3,4-dihydro-5-phenyl-2H-pyrano[3,2-c]quinolin-9-yl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C22H25NO3 → methyl 3-(3,4-dihydro-5-phenyl-2H-pyrano[3,2-c]quinolin-9-yl)propanoate (1185886-13-8)

Guidance literature:

C₂₂H₂₅NO₃; With triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In chloroform; for 3h; Reflux;

With palladium 10% on activated carbon; hydrogen; In ethanol; for 12h; under 760.051 Torr;

DOI:10.1021/jm900859q

Reference yield:

C22H25NO3 → C22H19NO3 + methyl 3-(3,4-dihydro-5-phenyl-2H-pyrano[3,2-c]quinolin-9-yl)propanoate (1185886-13-8)

Guidance literature:

With triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In chloroform; for 3h; Reflux;

DOI:10.1021/jm900859q

Reference yield:

methyl 3-(3,4-dihydro-5-phenyl-2H-pyrano[3,2-c]quinolin-9-yl)propanoate (1185886-13-8) → C21H19NO3*ClH (1185886-15-0)

Guidance literature:

methyl 3-(3,4-dihydro-5-phenyl-2H-pyrano[3,2-c]quinolin-9-yl)propanoate; With potassium hydroxide; In methanol; for 24h; Reflux;

With hydrogenchloride; In diethyl ether; for 0.5h;

DOI:10.1021/jm900859q

Downstream raw materials:

C₂₁H₁₉NO₃*ClH

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