(E)-1-[4-([D₃]methoxy)phenyl]-2-{4-[(trimethylsilyl)ethynyl]phenyl}diazene

Base Information

• Chemical Name: (E)-1-[4-([D₃]methoxy)phenyl]-2-{4-[(trimethylsilyl)ethynyl]phenyl}diazene
• CAS No.: 1253299-37-4
• Molecular Formula: C₁₈H₂₀N₂OSi
• Molecular Weight: 311.431

Synonyms:(E)-1-[4-([D₃]methoxy)phenyl]-2-{4-[(trimethylsilyl)ethynyl]phenyl}diazene

Chemical Property of (E)-1-[4-([D₃]methoxy)phenyl]-2-{4-[(trimethylsilyl)ethynyl]phenyl}diazene

Chemical Property:

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Technology Process of (E)-1-[4-([D₃]methoxy)phenyl]-2-{4-[(trimethylsilyl)ethynyl]phenyl}diazene

There total 1 articles about (E)-1-[4-([D₃]methoxy)phenyl]-2-{4-[(trimethylsilyl)ethynyl]phenyl}diazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

4-[(trimethylsilyl)ethynyl]nitrosobenzene + 4-([D3]methoxy)aniline (180626-23-7) → (E)-1-[4-([D3]methoxy)phenyl]-2-{4-[(trimethylsilyl)ethynyl]phenyl}diazene (1253299-37-4)

Guidance literature:

With acetic acid; for 16h;

DOI:10.1002/ejoc.201000650

Reference yield: 56.0%

(E)-1-[4-([D3]methoxy)phenyl]-2-{4-[(trimethylsilyl)ethynyl]phenyl}diazene (1253299-37-4) + 4,8,12-Tri-n-propyl-4,8,12-triazatriangulenium tetrafluoroborate → (E)-12c-{4-[4-([D3]methoxy)phenyldiazenyl]phenyl}ethynyl-4,8,12-tri-n-octyl-4,8,12-triazatriangulene (1253299-46-5)

Guidance literature:

(E)-1-[4-([D₃]methoxy)phenyl]-2-{4-[(trimethylsilyl)ethynyl]phenyl}diazene; With potassium hydroxide; In tetrahydrofuran; at 0 ℃; for 0.333333h; Inert atmosphere; Sonication;

4,8,12-Tri-n-propyl-4,8,12-triazatriangulenium tetrafluoroborate; In tetrahydrofuran; at 0 ℃; for 4h; Sonication;

DOI:10.1002/ejoc.201000650

upstream raw materials:

4-([D₃]methoxy)aniline

Downstream raw materials:

(E)-12c-{4-[4-([D₃]methoxy)phenyldiazenyl]phenyl}ethynyl-4,8,12-tri-n-octyl-4,8,12-triazatriangulene

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