methyl trans-3-(1-hydroxy-2-trityloxyethyl)-2,2-dimethylcyclopropanecarboxylate

Base Information

Chemical Name:methyl trans-3-(1-hydroxy-2-trityloxyethyl)-2,2-dimethylcyclopropanecarboxylate
CAS No.:764663-07-2
Molecular Formula:C₂₈H₃₀O₄
Molecular Weight:430.544
Hs Code.:

Synonyms:methyl trans-3-(1-hydroxy-2-trityloxyethyl)-2,2-dimethylcyclopropanecarboxylate

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Chemical Property of methyl trans-3-(1-hydroxy-2-trityloxyethyl)-2,2-dimethylcyclopropanecarboxylate

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Technology Process of methyl trans-3-(1-hydroxy-2-trityloxyethyl)-2,2-dimethylcyclopropanecarboxylate

There total 5 articles about methyl trans-3-(1-hydroxy-2-trityloxyethyl)-2,2-dimethylcyclopropanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 78646-25-0
4-dimethylamino-1-N-(triphenylmethyl)pyridinium chloride

: 120054-43-5
methyl trans-3-(1,2-dihydroxyethyl)-2,2-dimethylcyclopropanecarboxylate

: 764663-07-2
methyl trans-3-(1-hydroxy-2-trityloxyethyl)-2,2-dimethylcyclopropanecarboxylate

Guidance literature:: In dichloromethane; for 22h; Heating;
DOI:10.1016/j.tet.2004.06.035

Reference yield: 80.0%

: 120054-43-5
methyl trans-3-(1,2-dihydroxyethyl)-2,2-dimethylcyclopropanecarboxylate

: N,N-4-dimethylamino-N-triphenylmethylpyridinium tetrafluoroborate

: 764663-07-2
methyl trans-3-(1-hydroxy-2-trityloxyethyl)-2,2-dimethylcyclopropanecarboxylate

Guidance literature:: In acetonitrile; at 20 ℃; for 9h;
DOI:10.1016/j.tet.2004.06.035

Reference yield:

: 81703-94-8
methyl (2Z)-3-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]acrylate

: 764663-07-2
methyl trans-3-(1-hydroxy-2-trityloxyethyl)-2,2-dimethylcyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: LiI

2: 92 percent / aq. HCl / methanol / 0.5 h / 20 °C

3: 89 percent / CH₂Cl₂ / 22 h / Heating

With hydrogenchloride; lithium iodide; In methanol; dichloromethane;
DOI:10.1016/j.tet.2004.06.035