Technology Process of C30H46O7Si
There total 2 articles about C30H46O7Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / 0 - 20 °C
1.2: 2 h / 70 °C
2.1: dmap; water; sodium chloride / dimethyl sulfoxide / 19 h / 180 °C
3.1: bis-triphenylphosphine-palladium(II) chloride; tri-n-butyl-tin hydride / dichloromethane / 0.5 h / 20 °C
3.2: 1 h / 80 °C
With
dmap; bis-triphenylphosphine-palladium(II) chloride; water; tri-n-butyl-tin hydride; sodium hydride; sodium chloride;
In
tetrahydrofuran; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
2.1: Krapcho decarboalkoxylation / 3.2: Stille coupling;
DOI:10.1016/j.tetlet.2012.03.098
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 0.25 h / 20 °C
2.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / 0 - 20 °C
2.2: 2 h / 70 °C
3.1: dmap; water; sodium chloride / dimethyl sulfoxide / 19 h / 180 °C
4.1: bis-triphenylphosphine-palladium(II) chloride; tri-n-butyl-tin hydride / dichloromethane / 0.5 h / 20 °C
4.2: 1 h / 80 °C
With
dmap; bis-triphenylphosphine-palladium(II) chloride; carbon tetrabromide; water; tri-n-butyl-tin hydride; sodium hydride; triphenylphosphine; sodium chloride;
In
tetrahydrofuran; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
3.1: Krapcho decarboalkoxylation / 4.2: Stille coupling;
DOI:10.1016/j.tetlet.2012.03.098
